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Rapidly texturedBi2Sr2CaCu2O8

Published online by Cambridge University Press:  31 January 2011

S.R. Arrasmith ,
M.J. Kramer ,
B.D. Merkle ,
T.G. Holesinger  and
R.W. McCallum
S.R. Arrasmith
Affiliation:
Ames Laboratory, Iowa State University, Ames, Iowa 50011
M.J. Kramer
Affiliation:
Ames Laboratory, Iowa State University, Ames, Iowa 50011
B.D. Merkle
Affiliation:
Ames Laboratory, Iowa State University, Ames, Iowa 50011
T.G. Holesinger
Affiliation:
Argonne National Laboratory, Argonne, Illinois 60439
R.W. McCallum
Affiliation:
Ames Laboratory, Iowa State University, Ames, Iowa 50011
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Abstract

Amorphous Bi2Sr2CaCu2O8 (Bi-2212) was crystallized under uniaxial loads (up to 1500 N) at temperatures up to 890 °C to induce texture. Well-textured samples (19 mm in diameter and 0.15 mm thick) were obtained for samples heated to 890 °C and quenched. Heated (10 °C/min) and quenched samples at 550, 750, 850, and 870 °C demonstrate that the crystallization path is Bi2Sr2CuO6 (Bi-2201) (550 °C) to Bi-2212 (850 °C), with texturing occurring during grain growth (T > 850 °C). Comparison of samples crystallized under load and no load demonstrates that the texturing is a result of the plane stress biasing the normal anisotropic grain growth normal to the applied stress direction.

Type
Articles
Information
Journal of Materials Research , Volume 8 , Issue 6 , June 1993 , pp. 1247 - 1257
Copyright
Copyright © Materials Research Society 1993

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