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A Detailed Interface Characterization of the Explosively Welded Three-Layered Ti Gr 1/Alloy 400/1.4462 Steel Clads Before and After Heat Treatment

Published online by Cambridge University Press:  24 November 2021

Marta Janusz-Skuza Open the ORCID record for Marta Janusz-Skuza [Opens in a new window] ,
Agnieszka Bigos ,
Łukasz Maj ,
Jerzy Morgiel ,
Marek Faryna ,
Anna Sypien ,
Zygmunt Szulc  and
Joanna Wojewoda-Budka Open the ORCID record for Joanna Wojewoda-Budka [Opens in a new window]
Marta Janusz-Skuza*
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
Agnieszka Bigos
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
Łukasz Maj
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
Jerzy Morgiel
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
Marek Faryna
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
Anna Sypien
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
Zygmunt Szulc
Affiliation:
High Energy Technologies Works ‘Explomet’, 100H Oswiecimska St., 45-641 Opole, Poland
Joanna Wojewoda-Budka
Affiliation:
Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Cracow, Poland
*
*Corresponding author: Marta Janusz-Skuza, E-mail: m.janusz@imim.pl
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Abstract

The presented research focused on the microstructural characteristics of explosively welded three-layered Ti Grade (Gr) 1/Alloy 400/1.4462 steel clads before and after heat treatment being of large practical potential. Scanning electron microscopy (SEM) analyses have shown that both interfaces formed between the plates are continuous and without defects. The in-depth examination was dedicated to the upper Ti Gr 1/Alloy 400 interface, located closer to the explosive material, therefore, subjected to more extreme welding conditions. The presence of cubic phase Ti2Ni, hexagonal phase Ni3Ti, and tetragonal phase (CuxNi1−x)2Ti were confirmed within the melted zones, which slightly widened due to annealing, being an essential step in the manufacturing of these modern materials. Transmission electron microscopy observations in the nano scale confirmed the preliminary chemical composition analyses collected with energy-dispersive X-ray spectroscopy in SEM. They additionally revealed the interface zone microstructure transformation due to the annealing. It was evidenced that initially mixed phases in the form of grains, after heat treatment formed irregular bands arranged in the following sequence: Alloy 400/Ni3Ti/(CuxNi1−x)2Ti/Ti2Ni/Ti Gr 1. A clear segregation of Cu and Ni forming two separate layers was also noticed. These diffusion phenomena may influence the strength of the final product, therefore need further studies regarding the prolonged annealing state.

Keywords

explosive weldingheat treatmentinterfacemicrostructureSEM/TEM characterizationTi Gr 1/Alloy 400/1.4462 steel clads
Type
The XVIIth International Conference on Electron Microscopy (EM2020)
Information
Microscopy and Microanalysis , Volume 28 , Issue 3 , June 2022 , pp. 915 - 923
Copyright
Copyright © The Author(s), 2021. Published by Cambridge University Press on behalf of the Microscopy Society of America

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References

Bataev, IA, Lazurenko, DV, Tanaka, S, Hokamoto, K, Bataev, AA, Guo, Y & Jorge, AM Jr. (2017). High cooling rates and metastable phases at the interfaces of explosively welded materials. Acta Mater 135, 277–289.CrossRefGoogle Scholar
Bataev, IA, Ogneva, TS, Bataev, AA, Mali, VI, Esikov, MA, Lazurenko, DV, Guo, Y & Jorge Junior, AM (2015). Explosive welded multilayer Ni-Al composites. Mater Des 88, 1082–1087.CrossRefGoogle Scholar
Dobromyslov, AV & Taluts, NI (1987). Structure investigation of quenched and tempered alloys of the Zr-Ti system. Phys Met Metallogr 63, 114–120.Google Scholar
Durgutlu, A, Okuyucu, H & Gulenc, B (2008). Investigation of effect of the stand-off distance on interface characteristics of explosively welded copper and stainless steel. Mater Des 29, 1480–1484.CrossRefGoogle Scholar
Findik, F (2011). Recent developments in explosive welding. Mater Des 32, 1081–1093.CrossRefGoogle Scholar
Gargarella, P, Pauly, S, Song, KK, Hu, J, Barekar, NS, Samadi Khoshkhoo, M, Teresiak, A, Wendrock, H, Kuhn, U, Ruffing, C, Kerscher, E & Eckert, J (2013). Ti–Cu–Ni shape memory bulk metallic glass composites. Acta Mater 61, 151–162.CrossRefGoogle Scholar
Gladkovsky, SV, Kuteneva, SV & Sergeev, SN (2019). Microstructure and mechanical properties of sandwich copper/steel composites produced by explosive welding. Mater Charact 54, 294–303.CrossRefGoogle Scholar
Glimois, JL, Forey, P, Guillen, R & Féron, JL (1987). Structural study of the ternary alloys (Ti x Zr1−x)Ni. J. Less-Common Met 134, 221–228.CrossRefGoogle Scholar
Guo, X, Ma, Y, Jin, K, Wang, H, Tao, J & Fan, M (2017). Effect of standoff distance on the microstructure and mechanical properties of Ni/Al/Ni laminates prepared by explosive bonding. JMEPEG 26, 4235–4244.CrossRefGoogle Scholar
Kaçar, R & Acarer, M (2003). Microstructure–property relationship in explosively welded duplex stainless steel–steel. Mater Sci. Eng, A 363, 290–296.CrossRefGoogle Scholar
Kahraman, N, Gulenc, B & Findik, F (2007). Corrosion and mechanical-microstructural aspects of dissimilar joints of Ti–6Al–4 V and al plates. Int J Impact Eng 34, 1423–1432.CrossRefGoogle Scholar
Kwiecien, I, Bobrowski, P, Janusz-Skuza, M, Wierzbicka-Miernik, A, Tarasek, A, Szulc, Z & Wojewoda-Budka, J (2020). Interface characterization of Ni/Al bimetallic explosively welded plate manufactured with application of exceptionally high detonation speed. JMEPEG 29, 6286–6294.CrossRefGoogle Scholar
Liu, C, Zhang, YZ & Ye, L (2017). High velocity impact responses of sandwich panels with metal fibre laminate skins and aluminium foam core. Int J Impact Eng 100, 139–153.CrossRefGoogle Scholar
Naji, H, Khalil-Allafi, J & VK, (2020). Microstructural characterization and quantitative phase analysis of Ni-rich NiTi after stress assisted aging for long times using the Rietveld method. Mater Chem Phys 241, 122317.CrossRefGoogle Scholar
Neiman, AA, Semin, VO, Meisner, LL & Ostapenko, MG (2019). Structural decomposition and phase changes in TiNi surface layer modified by low-energy high-current pulsed electron beam. J Alloys Compd 803, 721–729.CrossRefGoogle Scholar
Paul, H, Chulist, R, Bobrowski, P, Perzynski, K, Madej, Ł, Mania, I, Miszczyk, M & Cios, G (2020). Microstructure and properties of the interface in explosive-welded and annealed titanium-copper sheets. Mater Charact 167, 110520.CrossRefGoogle Scholar
Radi, A, Khalil-Allafi, J, Etminanfar, MR, Pourbabak, S, Schryvers, D & Amin-Ahmadi, B (2018). Influence of stress aging process on variants of nano-Ni4Ti3 precipitates and martensitic transformation temperatures in NiTi shape memory alloy. Mater Des 142, 93–100.CrossRefGoogle Scholar
Raghavan, V (2012). Cu-Fe-Ni (copper-iron-nickel). J Phase Equilib Diffus 33, 232–235.CrossRefGoogle Scholar
Rejil, CM, Sharan, C, Muthukumaran, S & Vasudevan, M (2016). Influence of flash trap profiles on joint properties of friction welded CP-Ti tube to 304L stainless steel tube plate using external tool. Trans Nonferrous Met Soc China 26, 2067–2078.CrossRefGoogle Scholar
Sridharan, S, Nowotny, H & Wayne, SF (1983). Investigations within the quaternary system titanium-nickel-aluminium-carbon. Monatsh Chem 114, 127–135.CrossRefGoogle Scholar
Van Loo, FJJ, Basti, GF & Leenen, AJH (1978). Phase relations in the ternary Ti-Ni-Cu system at 800 and 870C. J Less-Common Met 57, 111–121.CrossRefGoogle Scholar
Zhou, Q, Liu, R, Chen, P & Zhu, L (2021). Microstructure characterization and tensile shear failure mechanism of the bonding interface of explosively welded titanium-steel composite. Mater Sci Eng, A 820, 141559.CrossRefGoogle Scholar
Zhu, WJ, Duarte, LI & Leinenbach, C (2014). Experimental study and thermodynamic assessment of the Cu–Ni–Ti system. CALPHAD: Comput Coupling Phase Diagrams Thermochem 47, 9–22.CrossRefGoogle Scholar