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In situ Observation of Compression Damage in a Three-Dimensional Braided Carbon Fiber Reinforced Carbon and Silicon Carbide (C/C-SiC) Ceramic Composite

Published online by Cambridge University Press:  19 June 2018

Fan Wan ,
Shixiang Zhao ,
Rongjun Liu ,
Changrui Zhang  and
Thomas J. Marrow
Fan Wan
Affiliation:
1Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, National University of Defense Technology, Changsha 410073, China 2Department of Materials, University of Oxford, Oxford OX1 3PH, UK
Shixiang Zhao
Affiliation:
2Department of Materials, University of Oxford, Oxford OX1 3PH, UK
Rongjun Liu
Affiliation:
1Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, National University of Defense Technology, Changsha 410073, China
Changrui Zhang
Affiliation:
1Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, National University of Defense Technology, Changsha 410073, China
Thomas J. Marrow*
Affiliation:
2Department of Materials, University of Oxford, Oxford OX1 3PH, UK
*
*Author for correspondence: Thomas James Marrow, E-mail: james.marrow@materials.ox.ac.uk
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Abstract

Deformation and mechanical damage in a three-dimensional braided carbon fiber reinforced carbon and silicon carbide ceramic composite, subjected to compressive loading, has been studied in situ by laboratory X-ray computed tomography. Dimensional change was measured and damage visualized by digital volume correlation analysis of tomographs. Cracks nucleated from defects within the fiber bundles and tended to propagate along the fiber bundle/matrix interface. For longitudinal compression, parallel to the fiber bundles, the initial elastic modulus decreased with increasing compressive strain while significant transverse tensile strains developed due to distributed cracking. For transverse compression, perpendicular to the fiber bundles, the compressive elastic modulus was effectively constant; the tensile strains developed along the fiber direction were small, whereas macroscopic fracture between the fiber bundles caused very large bulk tensile strain perpendicular to the loading. The observations suggest that the mechanical strength might be improved through control of pre-existing defects and application of stitch fibers in the transverse direction.

Keywords

C/C-SiCceramic compositecompression damageX-ray computed tomographydigital volume correlation
Type
Materials Science Applications
Information
Microscopy and Microanalysis , Volume 24 , Issue 3 , June 2018 , pp. 227 - 237
Copyright
© Microscopy Society of America 2018 

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Footnotes

Cite this article:Wan F, Zhao S, Liu R, Zhang C, Marrow TJ (2018) In situ Observation of Compression Damage in a Three-Dimensional Braided Carbon Fiber Reinforced Carbon and Silicon Carbide (C/C-SiC) Ceramic Composite. Microsc Microanal24(3): 227–237. doi: 10.1017/S1431927618000351

References

Arhatari, BD, Zonneveldt, M, Thornton, J Abbey, B (2017) Local structural damage evaluation of a C/C–SiC ceramic matrix composite. Microsc Microanal 23, 518–526.Google Scholar
Ashby, MF Hallam, SD (Née Cooksley) (1986) The failure of brittle solids containing small cracks under compressive stress states. Acta Metall 34, 497–510.Google Scholar
Barhli, SM, Saucedo-Mora, L, Jordan, MSL, Cinar, AF, Reinhard, C, Mostafavi, M Marrow, TJ (2017) Synchrotron X-ray characterization of crack strain fields in polygranular graphite. Carbon 124, 357–371.Google Scholar
Bay, BK, Smith, TS, Fyhrie, DP Saad, M (1999) Digital volume correlation: Three-dimensional strain mapping using X-ray tomography. Exp Mech 39, 217–226.CrossRefGoogle Scholar
Bažant, ZP Xiang, Y (1997) Size effect in compression fracture: Splitting crack band propagation. J Eng Mech 123, 162–172.Google Scholar
Bie, BX, Huang, JY, Fan, D, Sun, T, Fezzaa, K, Xiao, XH, Qi, ML Luo, SN (2017) Orientation-dependent tensile deformation and damage of a T700 carbon fiber/epoxy composite: A synchrotron-based study. Carbon 121, 127–133.Google Scholar
Bouterf, A, Roux, S, Hild, F, Adrien, J, Maire, E Meille, S (2014) Digital volume correlation applied to X-ray tomography images from spherical indentation tests on lightweight gypsum. Strain 50, 444–453.Google Scholar
Cai, B, Lee, PD, Karagadde, S, Marrow, TJ Connolley, T (2016) Time-resolved synchrotron tomographic quantification of deformation during indentation of an equiaxed semi-solid granular alloy. Acta Mater 105, 338–346.Google Scholar
Chen, Z, Fang, G, Xie, J Liang, J (2016) Experimental study of high-temperature tensile mechanical properties of 3D needled C/C–SiC composites. Mat Sci Eng A 654, 271–277.Google Scholar
Cui, YY, Bai, RC, Li, AJ, Ren, MS Sun, JL (2011) Microstructure and micromechanical property of C/C-SiC composites. Adv Mater Res 299–300, 238–241.CrossRefGoogle Scholar
Deng, J, Zhou, G, Ji, L Wang, X (2017) Mechanical behaviour of 3D multi-layer braided composites: Experimental, numerical and theoretical study. Appl Compos Mat 24, 1509–1523.CrossRefGoogle Scholar
Dongmei, Z, Hongna, D, Fa, L Wancheng, Z (2007) Preparation and mechanical properties of C/C-SiC composites. Mat Sci Forum 546–549, 1501–1504.Google Scholar
Emerson, MJ, Jespersen, KM, Dahl, AB, Conradsen, K Mikkelsen, LP (2017) Individual fibre segmentation from 3D X-ray computed tomography for characterising the fibre orientation in unidirectional composite materials. Compos Part A Appl Sci Manuf 97, 83–92.Google Scholar
Fan, X, Yin, X, Cao, X, Chen, L, Cheng, L Zhang, L (2015) Improvement of the mechanical and thermophysical properties of C/SiC composites fabricated by liquid silicon infiltration. Compos Sci Technol 115, 21–27.Google Scholar
Forsberg, F, Mooser, R, Arnold, M, Hack, E Wyss, P (2008) 3D micro-scale deformations of wood in bending: synchrotron radiation µCT data analyzed with digital volume correlation. J Struct Biol 164, 255–262.CrossRefGoogle Scholar
Forsberg, F Siviour, CR (2009) 3D deformation and strain analysis in compacted sugar using x-ray microtomography and digital volume correlation. Meas Sci Technol 20, 095703.Google Scholar
Gao, Y, Wang, Y, Yang, X, Liu, M, Xia, H, Huai, P Zhou, X (2016) Synchrotron X-ray tomographic characterization of CVI engineered 2D-woven and 3D-braided SiCf/SiC composites. Ceram Int 42, 17137–17147.CrossRefGoogle Scholar
Garcea, SC, Sinclair, I, Spearing, SM Withers, PJ (2017) Mapping fibre failure in situ in carbon fibre reinforced polymers by fast synchrotron X-ray computed tomography. Compos Sci Technol 149, 81–89.Google Scholar
Guvenilir, A, Breunig, TM, Kinney, JH Stock, SR (1997) Direct observation of crack opening as a function of applied load in the interior of a notched tensile sample of Al Li 2090. Acta Mater 45, 1977–1987.Google Scholar
Hodgkins, A, Marrow, TJ, Mummery, P, Marsden, B Fok, A (2006) X-ray tomography observation of crack propagation in nuclear graphite. Mater Sci Technol 22, 1045–1051.CrossRefGoogle Scholar
Hsu, TTC (1996) Toward a unified nomenclature for reinforced-concrete theory. J Struct Eng 122, 275–283.Google Scholar
Huang, L, Liu, R, Wang, Y, Zhang, C, Long, X Cao, Y (2016) Fabrication and properties of dense silicon carbide ceramic via gel-casting and gas silicon infiltration. Ceram Int 42, 18547–18553.Google Scholar
Joyce, MR, Marrow, TJ, Mummery, P Marsden, BJ (2008) Observation of microstructure deformation and damage in nuclear graphite. Eng Fract Mech 75, 3633–3645.CrossRefGoogle Scholar
Krenkel, W Berndt, F (2005) C/C–SiC composites for space applications and advanced friction systems. Mater Sci Eng A 412, 177–181.Google Scholar
Li, D-s, Lu, Z-x, Chen, L Li, J-l (2009) Microstructure and mechanical properties of three-dimensional five-directional braided composites. Int J Solids Struct 46, 3422–3432.Google Scholar
Li, D, Luo, G, Yao, Q, Jiang, N Jiang, L (2015) High temperature compression properties and failure mechanism of 3D needle-punched carbon/carbon composites. Mater Sci Eng A 621, 105–110.Google Scholar
Li, J-C, Chen, L, Zhang, Y-F Pan, N (2012) Microstructure and finite element analysis of 3D five-directional braided composites. J Reinf Plast Comp 31, 107–115.CrossRefGoogle Scholar
Marrow, TJ, Liu, D, Barhli, SM, Saucedo-Mora, L, Vertyagina, Y, Collins, DM, Reinhard, C, Kabra, S, Flewitt, PEJ Smith, DJ (2016) In situ measurement of the strains within a mechanically loaded polygranular graphite. Carbon 96, 285–302.CrossRefGoogle Scholar
Miyagawa, H, Mase, T, Sato, C, Drown, E, Drzal, LT Ikegami, K (2006) Comparison of experimental and theoretical transverse elastic modulus of carbon fibers. Carbon 44, 2002–2008.Google Scholar
Mostafavi, M, Bradley, R, Armstrong, DEJ Marrow, TJ (2016) Quantifying yield behaviour in metals by X-ray nanotomography. Sci Rep 6, 34346.CrossRefGoogle ScholarPubMed
Mostafavi, M, Collins, DM, Cai, B, Bradley, R, Atwood, RC, Reinhard, C, Jiang, X, Galano, M, Lee, PD Marrow, TJ (2015) Yield behavior beneath hardness indentations in ductile metals, measured by three-dimensional computed X-ray tomography and digital volume correlation. Acta Mater 82, 468–482.Google Scholar
Mostafavi, M, McDonald, SA, Mummery, PM Marrow, TJ (2013) Observation and quantification of three-dimensional crack propagation in poly-granular graphite. Eng Fract Mech 110, 410–420.Google Scholar
Nguyen, TT, Yvonnet, J, Bornert, M Chateau, C (2016) Initiation and propagation of complex 3D networks of cracks in heterogeneous quasi-brittle materials: Direct comparison between in situ testing-microCT experiments and phase field simulations. J Mech Phys Solids 95, 320–350. http://www.sciencedirect.com/science/article/pii/S0022509616302563.CrossRefGoogle Scholar
Nie, J, Xu, Y, Zhang, L, Fan, S, Xu, F, Cheng, L, Ma, J Yin, X (2010) Microstructure, thermophysical, and ablative performances of a 3D needled C/C-SiC composite. Int J Appl Ceram Technol 7, 197–206.Google Scholar
Nie, J, Xu, Y, Zhang, L, Yin, X, Cheng, L Ma, J (2008) Effect of stitch spacing on mechanical properties of carbon/silicon carbide composites. Compos Sci Technol 68, 2425–2432.Google Scholar
Park, HS, Jang, JJ, Lee, KH, Lim, KH, Park, SB, Kim, YC Hong, SH (2008) Effects of microstructure on flexural strength of biomorphic C/SiC composites. Int J Fract 151, 233–245.CrossRefGoogle Scholar
Poissant, J Barthelat, F (2010) A novel “subset splitting” procedure for digital image correlation on discontinuous displacement fields. Exp Mech 50, 353–364.Google Scholar
Réthoré, J, Limodin, N, Buffière, J-Y, Hild, F, Ludwig, W Roux, S (2011) Digital volume correlation analyses of synchrotron tomographic images. J Strain Anal Eng Des 46, 683–695.Google Scholar
Saucedo-Mora, L, Lowe, T, Zhao, S, Lee, PD, Mummery, PM Marrow, TJ (2016) In situ observation of mechanical damage within a SiC-SiC ceramic matrix composite. J Nucl Mater 481, 13–23.Google Scholar
Saucedo-Mora, L, Zou, C, Lowe, T Marrow, TJ (2017) Three-dimensional measurement and cohesive element modelling of deformation and damage in a 2.5-dimensional woven ceramic matrix composite. Fatigue Fract Eng Mater Struct 40, 683–695.Google Scholar
Schneider, CA, Rasband, WS Eliceiri, KW (2012) NIH Image to ImageJ: 25 years of image analysis. Nat Methods 9, 671.Google Scholar
Shih, C, Katoh, Y, Snead, LL Steinbeck, J (2013) The effect of neutron irradiation on the mechanical properties of C/SiC composites. J Nucl Mater 439, 192–201.Google Scholar
Steuwer, A, Edwards, L, Pratihar, S, Ganguly, S, Peel, M, Fitzpatrick, ME, Marrow, TJ, Withers, PJ, Sinclair, I, Singh, KD, Gao, N, Buslaps, T Buffière, J-Y (2006) In situ analysis of cracks in structural materials using synchrotron X-ray tomography and diffraction. Nucl Instrum Methods Phys Res B 246, 217–225.Google Scholar
Vertyagina, Y, Mostafavi, M, Reinhard, C, Atwood, R Marrow, TJ (2014) In situ quantitative three-dimensional characterisation of sub-indentation cracking in polycrystalline alumina. J Eur Ceram Soc 34, 3127–3232.Google Scholar
Wang, B, Jiao, GQ, Chang, YJ Pan, WG (2006) Shear and compress experimental study on 3-d braided C/Sic composites (in Chinese). J Aeronaut Mater 26, 64–67.Google Scholar
Wang, J, Lin, M, Xu, Z, Zhang, Y, Shi, Z, Qian, J, Qiao, G Jin, Z (2009) Microstructure and mechanical properties of C/C–SiC composites fabricated by a rapid processing method. J Eur Ceram Soc 29, 3091–3097.Google Scholar
Xie, J, Liang, J, Fang, G Chen, Z (2015) Effect of needling parameters on the effective properties of 3D needled C/C-SiC composites. Compos Sci Technol 117, 69–77.Google Scholar
Xiong, C, Li, T, Zhao, T, Khan, M, Wang, J, Ji, X, Li, H, Liu, W Shang, Y (2016) Preparation of C/C–SiC composite by low temperature compression molding–liquid silicon infiltration and its application in automobile brake. Ceram Int 42, 1057–1062.Google Scholar
Yang, Z, Ren, W, Sharma, R, McDonald, S, Mostafavi, M, Vertyagina, Y Marrow, TJ (2017) In-situ X-ray computed tomography characterisation of 3D fracture evolution and image-based numerical homogenisation of concrete. Cem Concr Compos 75, 74–83.Google Scholar
Zhang, D, Chen, L, Sun, Y Wang, X (2015) Transverse tensile damage behaviors of three-dimensional five-directional braided composites by meso-scale finite element approach. J Reinf Plast Comp 34, 1202–1220.Google Scholar
Zhou, X, Zhu, D, Xie, Q, Luo, F Zhou, W (2012) Friction and wear properties of C/C–SiC braking composites. Ceram Int 38, 2467–2473.Google Scholar