Published online by Cambridge University Press: 01 February 2011
We have observed the growth of defects caused by optical illumination in liquid nitrogen. We kept the sample in liquid nitrogen over one year. After one year and half the ESR signal reached ∼1018 cm−3 with no evidence of saturation. After that, we step-wise annealed isochronal the sample up to room temperature, where two thirds of original defects were annealed out. After room temperature, the sample was annealing isothermally around 300 K for several months. At this temperature, the defects slowly anneal. After a hundred of hours at 295K, the defect density decreased 10x from its original value at 77K.