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Published online by Cambridge University Press: 25 February 2011
MgO thin films were deposited on silicon and sapphire substrates using ion-beam reactive sputtering. Films have been analyzed using x-ray diffraction, transmission electron microscopy, and atomic force microscopy. Highly oriented (100) MgO films have been obtained on Si (100) substrates. The in-plane orientation is predominantly [100]MgO//[100]Si, although a twist of up to ±10° between grains is observed. Epitaxial films of MgO were deposited on four different orientations of sapphire. The MgO film orientation was (111) on c-cut (0001) Al2O3 and exhibited double positioning boundaries in TEM analysis. On r-cut (1102) Al2O3, the MgO appeared to be oriented (730) with tilt and twist of ±2° between the grains. Epitaxial MgO films oriented (110) and (111) were obtained on m-cut (1010) and a-cut (1120) sapphire orientations, respectively. In-plane directions were extracted from TEM analysis on all the samples. Atomic force microscopy revealed fairly smooth MgO films on sapphire, varying from 0.35 nm average roughness for the MgO film on the m-cut substrate to 0.80 nm on the r-cut substrate.