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Limiting Catalytic Coke Formation by the Application of Adherent SiC Coatings via Pulsed Laser Deposition to the Inner Diameter of Tube Material Traditionally Used for Ethylene Pyrolysis Service

Published online by Cambridge University Press:  01 February 2011

Alok Chauhan ,
Wilton Moran ,
Elizabeth Casey ,
Weidong Si  and
Henry White
Alok Chauhan
Affiliation:
Dept. of Materials Science, Stony Brook University, Stony Brook, New York 11794–2275
Wilton Moran
Affiliation:
Dept. of Materials Science, Stony Brook University, Stony Brook, New York 11794–2275
Elizabeth Casey
Affiliation:
Comsewogue High School, Port Jefferson Station, New York, 11776
Weidong Si
Affiliation:
Physics Department, Brookhaven National Laboratory, Upton, New York 11973–5000
Henry White
Affiliation:
Dept. of Materials Science, Stony Brook University, Stony Brook, New York 11794–2275
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Abstract

Pulsed laser deposited coatings can be used to enhance the corrosion resistant of materials traditionally used for industrial applications. In this paper, we describe our initial results on coating HK40 (a material used for ethylene heater tubing) with silicon carbide (a carburization resistant coating) to increase tube life. A 1 um thick film of silicon carbide was successfully deposited onto a heated HK40 substrate. An array of characterization techniques (scanning electron microscopy, atomic force microscopy, and scratch tests) demonstrated that the processing conditions were suitable for good coverage and promising adhesion behavior.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 843: Symposium T – Surface Engineering-Fundamentals and Applications , 2004 , T3.4
Copyright
Copyright © Materials Research Society 2005

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References

REFERENCES

[1] Mucek, M. W., “Laboratory Detection of Degree of Carburization in Ethylene Pyrolysis Furnace Tubing,” Materials Performance, 9, 25–28, 1983.Google Scholar
[2] Ropital, F., Sugier, A., Bisiaux, M., “Etude De La Restauration Des Caracteristiques De Tubes De Four De Vapocraquage En Manaurite 36XS,” Revue De L'Institut Francais Du Petrole, 44, 91–101, 1989.Google Scholar
[3] Ibarra, S., “Materials of Construction in Ethylene Pyrolysis- Heater Service,” In Pyrolysis: Theory & Industrial Practice, Albright, L. F., Crynes, B. L., Corcoran, W. H., Academic Press, 427–436, 1983.Google Scholar
[4] Hou, Q. R., Gao, J., Li, S. J., “Adherent SiC Coatings on Ni- Cr Alloys with a Composition- Graded Intermediate Layer,” Applied Physics A, 67, 367–370, 1998.Google Scholar
[5] Chen, M. Y., Murray, P. T., “Deposition and Characterization of SiC and Cordierite Thin Films by Pulsed Laser Evaporation,” Journal of Materials Science, 25, 4929–4932, 1990.Google Scholar
[6] Neri, F., Barreca, F., Trusso, S., “Excimer Laser Ablation of Silicon Carbide Ceramic Targets,” Diamond and Related Materials, 11, 273–279, 2002.Google Scholar
[7] Rimai, L., Ager, R., Logothetis, E. M., Weber, W. H., Hangas, J., “Preparation of Oriented Silicon Carbide Films by Laser Ablation of Ceramic Silicon Carbide Targets,” Applied Physics Letters, 59, 2266–2268, 1991.Google Scholar
[8] Steinmann, P. A., Tardy, Y., Hintermann, H. E., “Adhesion Testing by the Scratch Test Method: The Influence of Intrinsic and Extrinsic Parameters on the Critical Load,” Thin Solid Films, 154, 333–349, 1987.Google Scholar