Hostname: page-component-cd9895bd7-gbm5v Total loading time: 0 Render date: 2024-12-28T22:27:40.117Z Has data issue: false hasContentIssue false
  • English
  • Français

Phase transition of sigma-CrFe under fast electron irradiation

Published online by Cambridge University Press:  27 April 2015

T. Nagase ,
S. Anada ,
K. Kobayashi ,
H. Yasuda  and
H. Mori
T. Nagase
Affiliation:
Research Center for Ultra-High Voltage Electron Microscopy, Osaka University, 7-1, Mihogaoka, Ibaraki, Osaka 567-0047, Japan. Division of Materials and Manufacturing Science, Graduate School of Engineering, Osaka University, 2-1, Yamada-oka, Suita, Osaka 565-0871, Japan.
S. Anada
Affiliation:
Research Center for Ultra-High Voltage Electron Microscopy, Osaka University, 7-1, Mihogaoka, Ibaraki, Osaka 567-0047, Japan.
K. Kobayashi
Affiliation:
Research Center for Ultra-High Voltage Electron Microscopy, Osaka University, 7-1, Mihogaoka, Ibaraki, Osaka 567-0047, Japan.
H. Yasuda
Affiliation:
Research Center for Ultra-High Voltage Electron Microscopy, Osaka University, 7-1, Mihogaoka, Ibaraki, Osaka 567-0047, Japan. Division of Materials and Manufacturing Science, Graduate School of Engineering, Osaka University, 2-1, Yamada-oka, Suita, Osaka 565-0871, Japan.
H. Mori
Affiliation:
Research Center for Ultra-High Voltage Electron Microscopy, Osaka University, 7-1, Mihogaoka, Ibaraki, Osaka 567-0047, Japan.
Get access

Abstract

Preparation of a sigma-CrFe single-phase specimen was achieved by arc melting of pure Fe and Cr, cold rolling, and subsequent annealing at 973 K or 1073 K in vacuum. Cold rolling before annealing is effective for the annealing-induced formation of sigma-CrFe from the bcc solid-solution phase. The phase stability and the structural change from sigma-CrFe to a bcc solid-solution phase under fast electron irradiation were investigated by in situ transmission electron microscope (TEM) observation in the temperature range between 22 K and 473 K by using an ultra-high voltage electron microscope (UHVEM). The phase transition of sigma-CrFe by fast electron irradiation was found to occur at a particular temperature.

Keywords

metalcompoundmicrostructure
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1743: Symposium DD/WW – Materials and Radiation Effects for Advanced Nuclear Technologies , 2015 , mrsf14-1743-dd09-03
Copyright
Copyright © Materials Research Society 2015 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

Anada, S., Nagase, T., Kobayashi, K., Yasuda, H., and Mori, H., Acta Mater. 71, 195 (2014).CrossRefGoogle Scholar
Chen, S. L., Zhang, J. Y., Lu, X. G., Chou, K. C., and Chang, Y. A., J. Phase Equilib. Diffus. 27, 121 (2006).CrossRefGoogle Scholar
Takaoka, A., Ura, K., Mori, H., Katsuta, T., Matsui, I., and Hayashi, S., J. Electron Microsc. 46, 447 (1997).CrossRefGoogle Scholar
Chen, T. H. and Yang, J. R., Mater. Sci. Eng. A, 311, 28 (2001).CrossRefGoogle Scholar
Blenkinsop, P. A. and Nutting, J., J. Iron Steel Inst. 205, 953 (1967).Google Scholar
Tetsui, T., Shinohara, M., and Abiko, K., Phys. Stat. Sol. A 160, 459 (1997).3.0.CO;2-8>CrossRefGoogle Scholar
Dulis, E. J. and Smith, G. V., Met. Progr. 72, 193 (1952).Google Scholar
Garnieri, G. J., Miller, J., and Vawter, F., Trans. Am. Soc. Met. 42, 981 (1952).Google Scholar