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Quantitative Analysis of Sedimentary Minerals by Powder X-ray Diffraction

Published online by Cambridge University Press:  10 January 2013

Peter Bayliss
Affiliation:
Department of Geology and Geophysics University of Calgary, Alberta, Canada T2N 1N4

Abstract

The variables of reflection overlap, crystallinity and crystallite size, primary extinction, microabsorption, chemical substitutions, preferred orientation, and analytical procedures affect quantitative analysis by powder X-ray diffraction. The intensity of the strongest reflection (I) of 39 minerals from a typical sedimentary environment divided by the intensity of the strongest reflection (Ic) of corundum, I/Ic, may be used to determine mineral percentages. Because of the numerous variables mentioned above, the I/Ic ratios used should be taken from multi-mineral specimens that occur either in the same geological formation for quantitative analysis (±7%) or in a similar geological formation for quantitative analysis (±30%).

Type
Research Article
Copyright
Copyright © Cambridge University Press 1986

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