With a looming referendum on the secession of South Sudan, the drafters of the Abyei Arbitration Agreement were faced with a complex intra-state dispute and a limited time to resolve it. The parties to the dispute agreed on a procedural regime to govern the arbitration, combining both traditional and innovative provisions on procedural rules, the constitution of the tribunal, the schedule of pleadings, transparency, financing of the proceeding, and the role of the Permanent Court of Arbitration. This article examines the key provisions of the Abyei Arbitration Agreement and their implementation during the course of the arbitration, and evaluates the case's significance as procedural precedent for future intra- or inter-state arbitration. The article does not provide an analysis of the substantive findings of the tribunal.