Production and consumption of pottery tempered with fresh volcanic ash peaked in the Late to Terminal Classic periods in the Maya lowlands. Differences in the type of volcanic inclusion and vessel form indicate that the pottery was produced in multiple locations by different groups of potters. In this article, we characterize pottery from household contexts at Baking Pot, Belize, using thin-section petrography and neutron activation analysis (NAA) to document mineralogical and chemical variability and determine provenance. The pottery was produced by adding fresh volcanic ash to a micritic clay. The petrographic and chemical data indicate that this paste recipe was produced locally in the Belize Valley. Variation in the paste recipes used is likely due to both production differences and postdepositional alteration. We argue that it is critical to use both petrography and NAA to understand pottery production and provenance in the Maya region.

This article investigates the mechanisms by which different communities were articulated during the Late Intermediate period (ca. AD 1000–1450) in the Río Grande de San Juan Basin, also called the Chicha Region, located in the border region of Bolivia and Argentina. Through analyses of systems of pottery production, circulation, and consumption, we examine interaction networks, social integration, and alliance building at a regional level. Yavi-Chicha pottery from two sites in the Chicha Region—Chipihuayco, in the Talina Valley (Bolivia), and Finispatria, in San Juan Mayo (Argentina)—provide key insights into regional integration and constellations of practice through their localized technological style and shared consumption strategies. This study reveals that people of Finispatria incorporated the entire Yavi-Chicha-style household assemblage—partly produced in Chipihuayco, partly in Finispatria, or partly at some unknown location—into their everyday lives. We argue that the entire household ceramic repertoire of the study region played a fundamental and socially integrative role as it circulated across the region.

To evaluate the daily Se intake of 3- to 5-year-old Japanese children, we used seventy-two urine samples collected from fifty-three children (twenty-seven male and twenty-six female) from two cities in Miyagi prefecture, Japan. For measuring low Se concentrations with high precision, accuracy and rapidity in the 24-h urine samples, we developed an instrumental neutron activation analysis (INAA) method, that is without any chemical separation, using the short-lived 77mSe (t1/2 = 17·4 s) nuclide. The estimated Se intake of the fifty-three children was 51·5 (sd 30·2) µg/d (geometric mean: 42·7 µg/d). Ten subjects (three male and seven female), successfully provided 24-h urine samples over two or three consecutive days; their Se intake was 37·4 (sd 5·9) µg/d. Based on the logarithmically transformed data of these ten subjects, the ratio of intra-/inter-individual variances of usual Se intake was 16·7 (28·0/1·7) and geometric mean was 27·7 µg/d. The 5th to 95th percentile of usual Se intake of these ten subjects was 17·5 to 40·4 µg/d, which ranged between the recommended dietary allowance and tolerable upper intake level of Se by the Dietary Reference Intakes for Japanese (2015).

This study uses neutron activation analysis of ceramics to examine economic change and increasing social complexity at the Preclassic Maya site of Cahal Pech in Belize (1200 cal BC–cal AD 300). Seven compositional groups were identified from the site's civic-ceremonial centre and two peripheral residential groups. Analyses indicate that both utilitarian and non-utilitarian ceramics were locally produced as early as 1200 cal BC, and that by c. 700 cal BC, fineware vessels were being exported into neighbouring parts of Guatemala. These results provide direct evidence for economic interaction between Maya lowland communities and for their increasing socio-political complexity.

Thirty pyrite samples from a wide range of localities were analysed using relative comparator and k0 neutron activation analysis (NAA) techniques at the University of Missouri Research Reactor, Columbia, Missouri, USA (MURR) and the Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW, Australia (ANSTO), respectively. Statistical analyses of the trace-element data produced by the two methods showed a generally good correlation, with the majority of elemental concentrations of paired data reported by MURR and ANSTO being indistinguishable at a 0.05 significance level. Trace-element analyses of pyrite from Navajún in Spain by both techniques compare well with published data. There is evidence for contamination by Al, Na and Ti in one set of samples, this is likely to have been introduced by contact with a plastic used in sample preparation.

Low concentrations of elements in food can be measured with various techniques, mostly in small samples (mg). These techniques provide only reliable data when the element is distributed homogeneously in the material to be analysed either naturally or after a homogenisation procedure. When this is not the case or homogenisation fails, a technique should be applied that is able to measure in samples up to grams and even kilograms and regardless of the distribution of the element. An adaptation of neutron activation analysis (NAA), called large-sample NAA, has been developed and proven accurate and may be an attractive alternative in food research and mass balance studies. Like standard NAA, large-sample NAA can be used to measure both toxic and trace elements relevant for nutrition.

The discovery of the Nan'ao One shipwreck off the southern coast of China throws new light onto Chinese maritime trade during the late Ming period. The primary cargo was a massive consignment of blue-and-white export porcelain, most probably destined for markets in Southeast Asia or Europe. Compositional analysis was performed on 11 fragments of blue-and-white export porcelain from the wreck site and on 64 samples from 3 Chinese porcelain production centres. The results indicate that the blue-and-white export porcelain recovered from the Nan'ao One came from two sources: the Jingdezhen and Zhangzhou kilns. Given the location of the shipwreck, the most probable destinations were the Portuguese trading centre at Macau or the Dutch at Batavia.

The island of Cyprus was a major producer of copper and stood at the heart of east Mediterranean trade networks during the Late Bronze Age. It may also have been the source of the Red Lustrous Wheelmade Ware that has been found in mortuary contexts in Egypt and the Levant, and in Hittite temple assemblages in Anatolia. Neutron Activation Analysis (NAA) has enabled the source area of this special ceramic to be located in a geologically highly localised and geochemically distinctive area of western Cyprus. This discovery offers a new perspective on the spatial organisation of Cypriot economies in the production and exchange of elite goods around the eastern Mediterranean at this time.

Instrumental neutron activation analysis (NAA) was used to quantify the amounts of K, Mg, Cl, Ca and Mn leaked into water from imbibing dry seeds, dry fruits and isolated seed parts. A number of intact monocot and dicot dry seeds or fruits were studied as were some isolated parts such as testa, endosperm and embryo. All samples studied leaked detectable amounts of the five elements measured but the amounts leaked varied greatly. In most cases K was leaked in greater amounts than the other elements while Mn was leaked least. The leakage of Ca was highest from isolated seed coats and from mericarps of three umbelliferous species. Comparisons of the amount of element leaked with the total amount of that element present in the starting material showed that leakage, especially of K, represents a substantial loss of mineral nutrient reserves. The degree of leakage of elements did not appear to be closely related to the types of organic storage reserves present.

Zn is an essential mineral. The role of Zn in atherosclerosis is not clear. Epidemiological studies, which have reported contradictory results, are limited by the use of serum Zn levels as a marker of intake. We assessed the association of toenail Zn, which integrates dietary Zn intake over 3 to 12 months, with the risk of a first myocardial infarction. Toenail Zn concentrations were determined by neutron activation analysis in the European multi-centre case–control study on antioxidants, myocardial infarction and breast cancer. This multi-centre case–control study included 684 cases and 724 controls from eight European countries and Israel. Toenail Zn levels of controls (adjusted for age and study centre) were positively associated with age, α-tocopherol and Se, but not with additional dietary variables or with classical risk factors for CHD. Average toenail Zn was 106·0 mg/kg in cases (95 % CI 103·1, 108·9) and 107·5 mg/kg in controls (95 % CI 104·5, 110·7). After controlling for cardiovascular risk factors and for centre, the adjusted odds ratios of myocardial infarction for quintiles 2–5 of toenail Zn with respect to the first quintile were 0·97 (95 % CI 0·59, 1·58), 1·15 (95 % CI 0·72, 1·85), 0·91 (95 % CI 0·56, 1·50), and 0·85 (95 % CI 0·52, 1·39). The P for trend was 0·45. In conclusion toenail Zn levels (reflecting long-term dietary intake) were not significantly associated with acute myocardial infarction.