One of the most impressive examples of an Inca capacocha ceremony was discovered during an archaeological expedition to the summit of Misti volcano in 1998. The offerings at the site included several human sacrifices, along with fine ceramics and figurines made from gold, silver, and Spondylus sp. shell. One of the two burials appeared to contain the bones of males and the other of females. The sex was established based on the contents of the graves, because the fragile skeletal material had been badly affected by volcanic activity and exact identification was difficult to make in situ. To limit the risk of damage, the bones were excavated together with the surrounding soil and transported in frozen blocks to the Museo Santuarios Andinos of Universidad Católica de Santa María in Arequipa. This material was the object of a bioarchaeological investigation in February and March 2018. The results revealed that at least eight individuals had been buried in the graves. The findings have increased our understanding of the age categories and physical condition of the individuals chosen to be sacrificed during the capacocha ritual.