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Examination of Hard Segment and Soft Segment Phase Separation in Polyurethane Medical Materials by Electron Microscopy Techniques
Jennifer E. Taylor, Peter R. Laity, Steven S. Wong, Keith Norris, Peck Khunkamchoo, Martin Cable, Geoffrey Andrews, Anthony F. Johnson, Ruth E. Cameron
Journal:

Microscopy and Microanalysis / Volume 12 / Issue 2 / April 2006

Published online by Cambridge University Press:

09 December 2005, pp. 151-155

Print publication:

April 2006
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A combination of transmission electron microscopy (TEM) and in situ tensile testing in an environmental scanning electron microscopy (ESEM) was used to evaluate the static bulk and dynamic surface morphologies of medical polyurethanes. TEM results showed phase-separated hard segment and soft segment structures. Surface morphology as a function of strain was studied using ESEM in conjunction with a tensometer.

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Examination of Hard Segment and Soft Segment Phase Separation in Polyurethane Medical Materials by Electron Microscopy Techniques