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Construction of a Multimode High Resolution X-Ray Powder Diffractometer and its Perfomance

Published online by Cambridge University Press:  06 March 2019

Masayasu Kurahashi ,
Kazumasa Honda ,
Midori Goto ,
Yu Inari  and
Chuji Katayama
Masayasu Kurahashi
Affiliation:
National Chemical Laboratory for Industry Higashi 1-1, Tsukuba, Ibaraki, 305 Japan
Kazumasa Honda
Affiliation:
National Chemical Laboratory for Industry Higashi 1-1, Tsukuba, Ibaraki, 305 Japan
Midori Goto
Affiliation:
National Chemical Laboratory for Industry Higashi 1-1, Tsukuba, Ibaraki, 305 Japan
Yu Inari
Affiliation:
National Chemical Laboratory for Industry Higashi 1-1, Tsukuba, Ibaraki, 305 Japan
Chuji Katayama
Affiliation:
National Chemical Laboratory for Industry Higashi 1-1, Tsukuba, Ibaraki, 305 Japan
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Abstract

Recently some of the above authors determined the structure of an unsolved organic compound employing X-rays from a Synchrotron, an Imaging Plate, and a large radius camera. It would be more desirable if the high quality powder diffaction data could be obtained by a diffractometer or a camera of laboratory use. Therefore a multimode X-ray powder diffractometer which can be used for various experimental geometries such as Bragg-Brentano mode, Guinier mode and parallel beam mode was constructed in order to find the highest resolution geometry. In this paper wc present the results of the measurements employing these three modes.

Type
VI. XRD Instrumentation, Techniques and Reference Materials
Information
Advances in X-Ray Analysis , Volume 35 , Issue A: First Pacific-International Congress on X-ray Analytical Methods (PICXAM). Fortieth Annual Conference on Applications of X-ray Analysis, August 7-16, 1991 , 1991 , pp. 375 - 381
Copyright
Copyright © International Centre for Diffraction Data 1991

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References

1. Honda, K., Goto, M., and Kurahashi, M., Chem. Lett., 1990, 13–16 Google Scholar
2. Kurahashi, M. Honda, K. and Goto, M., Inari, Y. and Katayama, C., J. Appl. Cryst., 24(1991), 61–63 Google Scholar
3. Kosarev, E.L., Inverse Problem, 6(1990), 55–76 Google Scholar