Hostname: page-component-cd9895bd7-7cvxr Total loading time: 0 Render date: 2024-12-27T14:37:51.180Z Has data issue: false hasContentIssue false
  • English
  • Français

Julios: A Position-Sensitive Neutron Detector and its Application to White Beam Time-Of-Flight Diffraction

Published online by Cambridge University Press:  06 March 2019

G. Will ,
W. Schäfer  and
B. Jansen
G. Will
Affiliation:
Minora logical Institute, University Bonn Pcppclsdorfer Schloß, 53115 Bonn, Germany
W. Schäfer
Affiliation:
Minora logical Institute, University Bonn Pcppclsdorfer Schloß, 53115 Bonn, Germany
B. Jansen
Affiliation:
Minora logical Institute, University Bonn Pcppclsdorfer Schloß, 53115 Bonn, Germany
Get access

Extract

Position-sensitive detectors (PSD's) are commonly available for X-ray diffraction, where they are used in the angle dispersive mode at fixed wavelength λ. They are sensitive to the scattering angle 2Θ. The resolution of such instruments is determined by the physical properties of the detector, and, of course, the distance from the sample. Using continuous radiation solid state detectors (Ge, Ge(Li), Si(Li)) are sensitive to energy (equivalent to λ) at fixed scattering angle 2Θo, They are being used for X-rays, especially with synchrotron radiation. Because X-rays travel with the speed of light, those two techniques cannot be combined. Thermal neutrons, on the other hand, are comparatively slowly traveling particles (2200 m/s at 300 K) and consequently time-of-flight (TOF) instruments with choppers at continuous neutron beams are known for a long time; they are being used as well for diff-actomet! y as for inelastic scattering.

Type
Research Article
Information
Advances in X-Ray Analysis , Volume 37: Forty-Second Annual Conference on Applications of X-ray Analysis, August 2-6, 1993 , 1993 , pp. 375 - 384
Copyright
Copyright © International Centre for Diffraction Data 1993

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Bacon, G.E., 1975, ‘Neutron Diffraction”, Clarendon, Oxford.Google Scholar
Jansen, E., Schäfer, W., Szepesvary, A., Will, G. and Kurz, R., 1989, “The Solid State Scintillation PSD JULIOS”. Physica B 156&157: 584–587.Google Scholar
Jansen, E., Schäfer, W., Szepesvary, A., Will, G., Reinaitz, R., Müller, K.D., Tietze, H., and Stcigenbceger, U., 1991, “Position-sensitive Scintillation Detector JULIOS under Experimental Conditions at ISIS”, Physica B 180&181: 917–919.Google Scholar
Jansen, E.M., Siemes, H., Merz, P., Schäfer, W., Will. G. and Dahms, M., 1992, “Preferred Orientation of Experimentally Deformed Mt.Isa Chalcopyrite Ore”, Mineralogical Magazine 57: 45–53.Google Scholar
Kockelmann, W., Schäfer, W. and Will, G., 1991, “Neutron Diffraction Measurements on ErPO4 and ErVO4”, Eur. J. Solid State Inorg. Chem. 28: 515–518.Google Scholar
Kockelmann, W., Schäfer, W. and Will, G., 1992, “Low Temperature Neutron Diffraction Investigation of the Complex Incommensurate Magnetic Ordering Behaviour of TbAsO4”, J. Phys. Chem. Solids. 53: 913–921.Google Scholar
Schäfer, W., Jansen, E., Kurz, R. and Will, G., 1986, “The Jülich Linear Position-sensitive Scintillation Detector: Some Characteristics and Results”, Physica β 136: 110–113.Google Scholar
Schäfer, W., Jansen, E., Szepesvary, A., Skowronck, R., Will, G., Reinartz, R. and Müller, K.D., 1993b, “The Scintillation PSD JULIOS and its Use in TOP-Diffractometry at ISIS”, Proc. ICANS-XII, Abingdon, 24-28 May 1993, RAL-ReportGoogle Scholar
Schäfer, W., Jansen, E. and Will, G., 1993a, “Angle-dispersive Time-of-flight Diffraction in a Pulsed Beam”, J. Appl. Cryst. 26: in pritGoogle Scholar
Schäfer, W., Merz, P., Jansen, E. and Will, G., 1991. “Neutron Diffraction Texture Analysis of Multiphase and Low Symmetry Materials”, Textures and Microstructurcs 1-4: 65–71.Google Scholar
Schäfer, W., Will, G., Kotsanidis, P.A. and Yakinthos, J.K., 1990, “Magnetic Properties of RCoC2 (R = Y, Gd, Tb) Compounds”,. J. Magnetism and Magnetic Materials 88: 13–17.Google Scholar
Schäfer, W., Will, G., Yakinthos, J.K. and Kotsanidis, P.A., 1992, “Neutron Diffraction Study of RNiC2 (R = Rare Earth) Compounds”, J. Alloys and Compounds 180: 251–257.Google Scholar
Schelten, J., Kurz, R., Naday, I. and Schäfer, W., 1983, “Development of a Linear Position-sensitive Neutron Detector”, Nucl. Instrum. Meth. 205: 319–330.Google Scholar
Will, G., 1979, “POWLS: A Powder Least-squares Program”, J. Appl. Cryst. 12: 483–485.Google Scholar
Will, G., 1988, “Diffraction under Pressure with Synchrotron Radiation”, Zeitschrift f Kristalloge. 185; 100.Google Scholar