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A combustion synthesis process for synthesizing nanocrystalline zirconia powders

Published online by Cambridge University Press:  03 March 2011

K.R. Venkatachari ,
Dai Huang ,
Steven P. Ostrander ,
Walter A. Schulze  and
Gregory C. Stangle
K.R. Venkatachari
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Dai Huang
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Steven P. Ostrander
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Walter A. Schulze
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Gregory C. Stangle
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
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Abstract

Materials with nanocrystalline features are expected to have improved or unique properties when compared to those of conventional materials. Methods for the practical and economical production of nanoparticles in large quantities are not presently available. A method based on combustion synthesis for preparing nanocrystalline powders was investigated in this work. Yttria-doped zirconia powders with an average crystallite size of 10 nm were synthesized. The characteristics of the powder (e.g., surface area and phase content) were found to depend strongly on the fuel content in the starting mixture and on the ignition temperature used in the process. The method is expected to be suitable for commercial fabrication of nanocrystalline multicomponent oxide ceramic powders.

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Articles
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Journal of Materials Research , Volume 10 , Issue 3 , March 1995 , pp. 748 - 755
Copyright
Copyright © Materials Research Society 1995

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