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A combustion synthesis process for synthesizing nanocrystalline zirconia powders

Published online by Cambridge University Press:  03 March 2011

K.R. Venkatachari
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Dai Huang
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Steven P. Ostrander
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Walter A. Schulze
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
Gregory C. Stangle
Affiliation:
School of Ceramic Engineering and Sciences, New York State College of Ceramics at Alfred University, Alfred, New York 14802
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Abstract

Materials with nanocrystalline features are expected to have improved or unique properties when compared to those of conventional materials. Methods for the practical and economical production of nanoparticles in large quantities are not presently available. A method based on combustion synthesis for preparing nanocrystalline powders was investigated in this work. Yttria-doped zirconia powders with an average crystallite size of 10 nm were synthesized. The characteristics of the powder (e.g., surface area and phase content) were found to depend strongly on the fuel content in the starting mixture and on the ignition temperature used in the process. The method is expected to be suitable for commercial fabrication of nanocrystalline multicomponent oxide ceramic powders.

Type
Articles
Copyright
Copyright © Materials Research Society 1995

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References

REFERENCES

1Gleiter, H., Prog. Mater. Sci. 33, 223315 (1989).CrossRefGoogle Scholar
2Kear, B. H., Cross, L. E., Keem, J. E., Siegel, R. W., Spaipen, F., Taylor, K. C., Thomas, E. L., and Tu, K. N., Research Opportunities for Materials with Ultrafine Microstructures, National Materials Advisory Board–454 (National Academy Press, Washington, DC, 1989).Google Scholar
3Multicomponent Ultrafine Microstructures, edited by Mc-Candlish, L.E., Polk, D. E., Siegel, R. W., and Kear, B. H. (Mater. Res. Soc. Symp. Proc. 132, Pittsburgh, PA, 1989).Google Scholar
4Aksay, I. A., Han, C., Maupin, G. D., Martin, C. B., Kurosky, R. P., and Stangle, G. C., US Patent No. 5,061,682, Oct. 1991.Google Scholar
5Ravindranathan, P. and Patil, K. C., Am. Ceram. Soc. Bull. 66 (4), 688692 (1987).Google Scholar
6Kingsley, J. J. and Patil, K. C., Mater. Lett. 6 (11–12), 427432 (1988).CrossRefGoogle Scholar
7Chick, L. A., Bates, J. L., Peterson, I. R., and Kissinger, H. E., Proc. 1st Int. Symp. on Solid Oxide Fuel Cells, edited by Singhal, S. C. (The Electrochemical Society, Pennington, NJ, 1989), pp. 170187.Google Scholar
8Kourtakis, K., Robbins, M., Gallagher, P. K., and Tiefel, T., J. Mater. Res. 4 12891291 (1989).Google Scholar
9Chambers, C. and Holliday, A. K., Modern Inorganic Chemistry (Butterworth & Co., Ltd., London, 1975), pp. 242243.Google Scholar
10Klug, H. and Alexander, L., X-ray Diffraction Procedures (Wiley, New York, 1962).Google Scholar
11Beckstead, M. W., Derr, R. L., and Price, C. F., Proc. 13th Symp. (Int.) on Combustion (The Combustion Institute, Pittsburgh, PA, 1971).Google Scholar
12Phase Diagrams for Ceramists, edited by Roth, R. S., Dennis, J. R., and McMurdie, H. F. (The American Ceramic Society, Westerville, OH, 1987), Vol. VI.Google Scholar
13Kingery, W. D., Bowen, H. K., and Uhlmann, D. R., Introduction to Ceramics, 2nd ed. (John Wiley & Sons, New York, 1976), pp. 182183.Google Scholar
14Sōmiya, S., Yoshimura, M., Nakai, Z., Hishinuma, K., and Kumaki, T., in Advances in Ceramics, Ceramic Powder Science, edited by Messing, G. L., Mazdiyasni, K. S., McCauley, J. W., and Haber, R. A. (The American Ceramic Society, Westerville, OH, 1987), Vol. 21, pp. 4356.Google Scholar
15Foster, C. M., Bai, G. R., Parker, J. C., and Ali, M. N., in Nanophase and Nanocomposite Materials, edited by Komarneni, S., Parker, J. C., and Thomas, G. J. (Mater. Res. Soc. Symp. Proc. 286, Pittsburgh, PA, 1993), pp. 6166.Google Scholar
16Zhang, Y. and Stangle, G. C., J. Mater. Res. 8, 17031711 (1993).Google Scholar
17Russel, W. B., The Dynamics of Colloidal Systems (The University of Wisconsin Press, 1987), pp. 3942.Google Scholar
18Venkatachari, K. R., Huang, D., Ostrander, S. P., Schulze, W. A., and Stangle, G. C., J. Mater. Res. 10, 756761 (1995).Google Scholar
19Sekar, M.M. A. and Patil, K.C., J. Mater. Chem. 2 (7), 739743 (1992).Google Scholar
20Masters, K., Spray Drying Handbook (John Wiley & Sons, New York, 1979).Google Scholar