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Dependence of microstructure characteristics and mechanical properties on nanosize SiCp contents in Mg–9Al matrix composites fabricated by ultrasonic-assisted semisolid powder hot pressing

Published online by Cambridge University Press:  21 June 2018

Gang Li ,
Ming Li ,
Hongxia Wang ,
Zengyao Zhang ,
Weili Cheng ,
Wei Liang  and
Changjiang Zhang
Gang Li
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
Ming Li
Affiliation:
Southwest Technology and Engineering Research Institute, Precision Forming Center, Chongqing 400039, People’s Republic of China
Hongxia Wang*
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
Zengyao Zhang
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
Weili Cheng
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
Wei Liang
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
Changjiang Zhang
Affiliation:
Shanxi Key Laboratory of Advanced Magnesium Based Materials, College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
*
a)Address all correspondence to this author. e-mail: wanghxia1217@163.com
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Abstract

Nanosize SiCp (n-SiCp) reinforced Mg–9Al matrix composites (Mg–9Al–xSiC, x = 2.5, 5, 7.5, 10 wt%) with nearly full densification are fabricated by the semisolid powder hot pressing technique assisted with ultrasonic. The effect of SiC nanoparticle contents on microstructures and mechanical properties of the composites is systematically investigated. Grain size and density of Mg–9Al–xSiC composites and morphology of bonding interfacial between the n-SiCp and matrix are found to be greatly dependent on the n-SiCp contents, resulting in the strength and ductility of the composites increase first and then decrease as the increase of n-SiCp contents. As the SiCp content increasing to 7.5 wt%, superior mechanical properties with the yield strength of 191 MPa, ultimate tensile strength of 248 MPa, and elongation to failure of 5.3% are achieved. The improved mechanical properties could be attributed to grain boundary strengthening, Orowan strengthening, and load transfer strengthening.

Keywords

magnesium matrix compositessemisolid powder hot pressingmicrostructuremechanical propertiesstrengthening mechanism
Type
Article
Information
Journal of Materials Research , Volume 33 , Issue 18 , 28 September 2018 , pp. 2689 - 2699
Copyright
Copyright © Materials Research Society 2018 

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References

REFERENCES

Esmaily, M., Mortazavi, N., Svensson, J.E., Halvarsson, M., Wessén, M., Johansson, L.G., and Jarfors, A.E.W.: A new semi-solid casting technique for fabricating SiC-reinforced Mg alloys matrix composites. Composites, Part B 94, 176–189 (2016).CrossRefGoogle Scholar
Poddar, P., Srivastava, V.C., De, P.K., and Sahoo, K.L.: Processing and mechanical properties of SiC reinforced cast magnesium matrix composites by stir casting process. Mater. Sci. Eng., A 460–461, 357–364 (2007).CrossRefGoogle Scholar
Chen, Q., Chen, G., Han, F., Xia, X.S., and Wu, Y.: Microstructures, mechanical properties, and wear resistances of thixoextruded SiCp/WE43 magnesium matrix composites. Metall. Mater. Trans. A 48, 3497–3513 (2017).CrossRefGoogle Scholar
Mallick, A., Tun, K.S., and Gupta, M.: Deformation behaviour of Mg/Y2O3 nanocomposite at elevated temperatures. Mater. Sci. Eng., A 551, 222–230 (2012).CrossRefGoogle Scholar
Lelito, J., Zak, P.L., Shirzadi, A.A., Greer, A.L., Krajewski, W.K., Suchy, J.S., Haberl, K., and Schumacher, P.: Effect of SiC reinforcement particles on the grain density in a magnesium-based metal–matrix composite: Modelling and experiment. Acta Mater. 60, 2950–2958 (2012).CrossRefGoogle Scholar
Mirshahi, F. and Meratian, M.: High temperature tensile properties of modified Mg/Mg2Si in situ composite. Mater. Des. 33, 557–562 (2012).CrossRefGoogle Scholar
Wang, X.J., Xu, D.K., and Wu, R.Z.: What is going on in magnesium alloys? J. Mater. Sci. Technol. 34, 245–247 (2018).CrossRefGoogle Scholar
Jarry, P., Laurent, V., and Regazzoni, G.: Processing-microstructure relationships in compocast magnesium/SiC. J. Mater. Sci. 27, 4447–4459 (1992).Google Scholar
Huang, S.J., Jeng, Y.R., Semenov, V.I., and Dai, Y.Z.: Particle size effects of silicon carbide on wear behavior of SiCp-reinforced magnesium matrix composites. Tribol. Lett. 42, 79–87 (2011).CrossRefGoogle Scholar
Wang, Z.G., Li, C.P., Wang, H.Y., Zhu, X., Wu, M., and Jiang, Q.C.: Effect of nano-SiC content on mechanical properties of SiC/2014Al composites fabricated by powder metallurgy combined with hot extrusion. Powder Metall. 59, 236–241 (2016).CrossRefGoogle Scholar
Luo, D., Pei, C.H., Rong, J., Wang, H.Y., Li, Q., and Jiang, Q.C.: Microstructure and mechanical properties of SiC particles reinforced Mg–8Al–1Sn magnesium matrix composites fabricated by powder metallurgy. Powder Metall. 58, 349–353 (2016).CrossRefGoogle Scholar
Shen, M.J., Wang, X.J., Zhang, M.F., Hu, X.S., Zheng, M.Y., and Wu, K.: Fabrication of bimodal size SiCp reinforced AZ31B magnesium matrix composites. Mater. Sci. Eng., A 601, 58–64 (2014).CrossRefGoogle Scholar
Nie, K.B., Wang, X.J., Hu, X.S., Xu, L., Wu, K., and Zheng, M.Y.: Microstructure and mechanical properties of SiC nanoparticles reinforced magnesium matrix composites fabricated by ultrasonic vibration. Mater. Sci. Eng., A 528, 5278–5282 (2011).CrossRefGoogle Scholar
Yao, X., Zhang, Z., and Zheng, Y.F.: Effects of SiC nanoparticle content on the microstructure and tensile mechanical properties of ultrafine grained AA6063-SiCnp nanocomposites fabricated by powder metallurgy. J. Mater. Sci. Technol. 9, 1023–1030 (2017).CrossRefGoogle Scholar
Kang, Y.C. and Chan, L.I.: Tensile properties of nanometric Al2O3 particulate-reinforced aluminum matrix composites. Mater. Chem. Phys. 85, 438–443 (2004).CrossRefGoogle Scholar
Shen, M.J., Wang, X.J., Ying, T., Wu, K., and Song, W.J.: Characteristics and mechanical properties of magnesium matrix composites reinforced with micron/submicron/nano SiC particles. J. Alloys Compd. 686, 831–840 (2016).CrossRefGoogle Scholar
Zhou, S.S., Deng, K.K., Li, J.C., Shang, S.J., Liang, W., and Fan, J.F.: Effects of volume ratio on the microstructure and mechanical properties of particle reinforced magnesium matrix composite. Mater. Des. 63, 672–677 (2014).CrossRefGoogle Scholar
Xiong, G., Nie, Y., Ji, D., Li, J., Li, C., Li, W., Zhu, Y., Luo, H., and Wan, Y.: Characterization of biomedical hydroxyapatite/magnesium composites prepared by powder metallurgy assisted with microwave sintering. Curr. Appl. Phys. 16, 830–836 (2016).CrossRefGoogle Scholar
Yu, H., Sun, Y., Hu, L., Zhou, H., and Wan, Z.: Microstructural evolution of AZ61–10 at.% Ti composite powders during mechanical milling. Mater. Des. 104, 265–275 (2016).CrossRefGoogle Scholar
Hou, L.G., Wu, R.Z., Wang, X.D., Zhang, J.H., Zhang, M.L., Dong, A.P., and Sun, B.D.: Microstructure, mechanical properties and thermal conductivity of the short carbon fiber reinforced magnesium matrix composites. J. Alloy. Comp. 695, 2820–2826 (2016).CrossRefGoogle Scholar
Wang, E. and Hu, L.X.: Fabrication and mechanical properties of SiCw:ZK51A magnesium matrix composite by two-step squeeze casting. Mater. Sci. Eng., A 278, 267–271 (2000).Google Scholar
Wu, K., Zheng, M.Y., and Yao, C.K.: Effect of interfacial reaction on mechanical behavior of SiCw/AZ91 magnesium matrix composite. Mater. Sci. Eng., A 318, 50–56 (2001).Google Scholar
Deng, K.K., Wang, X.J., Wang, C.J., Shi, J.Y., Hu, X.S., and Wu, K.: Effects of bimodal size SiC particles on the microstructure evolution and fracture mechanism of AZ91 matrix at room temperature. Mater. Sci. Eng., A 553, 74–79 (2012).CrossRefGoogle Scholar
Deng, K., Wang, C., Wang, X., Wu, K., and Zheng, M.: Microstructure and elevated tensile properties of submicron SiCp/AZ91 magnesium matrix composite. Mater. Des. 38, 110–114 (2012).CrossRefGoogle Scholar
Chen, Q., Chen, G., Han, L.N., Hu, N., Han, F., Zhao, Z.D., Xia, X.S., and Wan, Y.Y.: Microstructure evolution of SiCp/ZM6 (Mg–Nd–Zn) magnesium matrix composite in the semi-solid state. J. Alloys Compd. 656, 67–76 (2016).CrossRefGoogle Scholar
Li, M., Wang, H., and Nie, K.: Microstructure and tensile properties of n-SiCp/Mg–9% Al composites prepared by ultrasonic assisted hot pressing of powder. J. Mater. Eng. Perform. 26, 1847–1855 (2017).CrossRefGoogle Scholar
Chen, C., Guo, L., and Luo, J.: Aluminum powder size and microstructure effects on properties of boron nitride reinforced aluminum matrix composites fabricated by semi-solid powder metallurgy. Mater. Sci. Eng., A 646, 306–314 (2015).CrossRefGoogle Scholar
Chen, H.S., Wang, W.X., and Li, Y.L.: The design, microstructure and mechanical properties of B4C/6061Al neutron absorber composites fabricated by SPS. Mater. Des. 94, 360–367 (2016).CrossRefGoogle Scholar
Mondet, M., Barraud, E., and Lemonnier, S.: Microstructure and mechanical properties of AZ91 magnesium alloy developed by Spark Plasma Sintering. Acta Mater. 119, 55–67 (2016).CrossRefGoogle Scholar
Luo, D., Wang, H.Y., and Zhang, L.: Microstructure evolution and tensile properties of hot rolled Mg–6Al–3Sn alloy sheet at elevated temperatures. Mater. Sci. Eng., A 643, 149–155 (2015).CrossRefGoogle Scholar
Jiang, J. and Wang, Y.: Microstructure and mechanical properties of the semisolid slurries and rheoformed component of nano-sized SiC/7075 aluminum matrix composite prepared by ultrasonic-assisted semisolid stirring. Mater. Sci. Eng., A 639, 350–358 (2015).CrossRefGoogle Scholar
Guan, H.R., Sun, B.W., and Sun, X.F.: A model of metal-oxide diffusion barrier. Acta Metall. Sin. 27, 108–113 (1990).Google Scholar
Shen, M.J., Ying, T., Chen, F.Y., and Hou, J.M.: Effect of micro- and nano-SiC particulate reinforcements in magnesium-based metal matrix composites. J. Mater. Eng. Perform. 25, 2222–2229 (2016).CrossRefGoogle Scholar
Wang, H.W., Wang, X.H., Liu, M.Y., Nie, H.H., and Cheng, L.W.: Effect of SiC nanoparticles addition on the microstructures and mechanical properties of ECAPed Mg9Al–1Si alloy. J. Mater. Res. 32, 615–623 (2017).CrossRefGoogle Scholar
Lu, L., Chua, B.W., and Lai, M.O.: Influence of SiC particles on mechanical properties of Mg based composite. Compos. Struct. 47, 595–601 (1999).Google Scholar
Cao, G., Choi, H., Konishi, H., Kou, S., Lakes, R., and Li, X.: Mg–6Zn/1.5% SiC nanocomposites fabricated by ultrasonic cavitation-based solidification processing. J. Mater. Sci. 43, 5521–5526 (2008).CrossRefGoogle Scholar
Erman, A., Groza, J., Li, X., Choi, H., and Cao, G.: Nanoparticle effects in cast Mg–1 wt% SiC nano-composites. Mater. Sci. Eng., A 558, 39–43 (2012).CrossRefGoogle Scholar
Lee, D.M., Suh, B.K., Kim, B.G., Lee, J.S., and Lee, C.H.: Fabrication, microstructures, and tensile properties of magnesium alloy AZ91/SiCp composites produced by powder metallurgy. Mater. Sci. Technol. 13, 590–595 (2013).CrossRefGoogle Scholar
Chen, L.Y., Xu, J.Q., Choi, H., Pozuelo, M., Ma, X., Bhowmick, S., Yang, J.M., Mathaudhu, S., and Li, X.C.: Processing and properties of magnesium containing a dense uniform dispersion of nanoparticles. Nature 528, 539–543 (2015).CrossRefGoogle ScholarPubMed
Zhang, Z. and Chen, D.L.: Consideration of Orowan strengthening effect in particulate-reinforced metal matrix nanocomposites: A model for predicting their yield strength. Scripta Mater. 54 7, 1321–1326 (2006).CrossRefGoogle Scholar
Hou, L., Cheng, L.B., Wu, R.Z., Cui, L., Ji, P., Long, R.Y., Zhang, J.H., Li, X.L., Dong, A.P., and Sun, B.D.: Microstructure and mechanical properties at elevated temperature of Mg–AI–Ni alloys prepared through powder metallurgy. J. Mater. Sci. Technol. 33, 947–953 (2017).CrossRefGoogle Scholar
Wu, L.G., Wu, R.Z., Hou, L., Zhang, J.H., Sun, J.F., and Zhang, M.L.: Microstructure and mechanical properties of CNT-reinforced AZ31 matrix composites prepared using hot-press sintering. J. Mater. Eng. Perform., 26, 1–6 (2017).CrossRefGoogle Scholar