Hostname: page-component-78c5997874-g7gxr Total loading time: 0 Render date: 2024-11-11T09:07:46.915Z Has data issue: false hasContentIssue false

Damage behavior of Cu–Ta bilayered films under cyclic loading

Published online by Cambridge University Press:  31 January 2011

X.F. Zhu
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People’s Republic of China
G.P. Zhang*
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People’s Republic of China
J. Tan
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People’s Republic of China
Y. Liu
Affiliation:
Nanometrics Inc., Milpitas, California 95035
S.J. Zhu
Affiliation:
Department of Intelligent Mechanical Engineering, Fukuoka Institute of Technology, Higashi-ku, Fukuoka, 811-0295, Japan
*
a)Address all correspondence to this author.e-mail: gpzhang@imr.ac.cn
Get access

Abstract

Damage behavior of Cu–Ta bilayered films bonded to polyimide (PI) substrates has been investigated by cyclic loading tests. Experimental results show that fatigue cracks preferentially initiated in the Ta layer close to the Ta–PI interface and propagated into the Cu layer perpendicular to the interface. The alignment of nanometer-sized Cu grains resulted from the potential GB sliding combined with a small amount of grain rotation was found in the damage zone ahead of the crack tip, and that is suggested to be a likely damage mechanism to accommodate cyclic plastic strain ahead of the fatigue crack tip of the submicrometer-thick Cu layer.

Type
Articles
Copyright
Copyright © Materials Research Society 2007

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1Nix, W.D.: Mechanical properties of thin films. Metall. Trans. A 20, 2217 1989CrossRefGoogle Scholar
2Arzt, E.: Size effects in materials due to microstructural and dimensional constraints: A comparative review. Acta Mater. 46, 5611 1998CrossRefGoogle Scholar
3Suresh, S.: Fatigue of Materials Cambridge University Press Cambridge 1999 44Google Scholar
4Schwaiger, R., Dehm, G.Kraft, O.: Cyclic deformation of polycrystalline Cu films. Philos. Mag. 83, 693 2003CrossRefGoogle Scholar
5Zhang, G.P., Volkert, C.A., Schwaiger, R., Wellner, P., Arzt, E.Kraft, O.: Length-scale-controlled fatigue mechanisms in thin copper films. Acta Mater. 54, 3127 2006CrossRefGoogle Scholar
6Zhang, G.P., Volkert, C.A., Schwaiger, R., Arzt, E.Kraft, O.: Damage behavior of 200-nm thin copper films under cyclic loading. J. Mater. Res. 20, 201 2005CrossRefGoogle Scholar
7Misra, A., Kung, H., Hammon, D., Hoagland, R.G.Nastasi, M.: Damage mechanisms in nanolayered metallic composites. Int. J. Damg. Mech. 12, 365 2003CrossRefGoogle Scholar
8Wang, Y.C., Misra, A.Hoagland, R.G.: Fatigue properties of nanoscale Cu/Nb multilayers. Scripta Mater. 54, 1593 2006CrossRefGoogle Scholar
9Zhang, G.P., Zhu, X.F., Tan, J.Liu, Y.: Origin of cracking in nanoscale Cu–Ta multilayers. Appl. Phys. Lett. 89, 041920 2006CrossRefGoogle Scholar
10Catania, P., Roy, R.A.Cuomo, J.J.: Phase formation and microstructure changes in tantalum thin films induced by bias sputtering. J. Appl. Phys. 72, 1008 1993CrossRefGoogle Scholar
11Ren, H.Sosnowski, M.: Effect of ion irradiation on α and β phase evolution of sputtered tantalum thin films in Thermodynamics and Kinetics of Phase Transformations in Inorganic Materials, edited by C. Ambromeit, P. Bellon, J-L. Bocquet, and D.N. Seidman Mater. Res. Soc. Symp. Proc. 979E, Warrendale, PA 2007 HH11-09Google Scholar
12Hanlon, T., Tabachnikova, E.D.Suresh, S.: Fatigue behavior of nanocrystalline metals and alloys. Int. J. Fatigue 27, 1147 2005CrossRefGoogle Scholar
13Farkas, D., Willemann, M.Hyde, B.: Atomistic mechanisms of fatigue in nanocrystalline metals. Phys. Rev. Lett. 94, 165502 2005CrossRefGoogle ScholarPubMed
14Hattar, K., Han, J., Saif, M.T.A.Robertson, I.M.: In situ transmission electron microscopy observations of toughening mechanisms in ultra-fine grained columnar aluminum thin films. J. Mater. Res. 20, 1869 2005CrossRefGoogle Scholar
15Schiøtz, J., Ditolla, F.D.Jacobsen, K.W.: Softening of nanocrystalline metals at very small grain sizes. Nature 391, 561 1998CrossRefGoogle Scholar
16Meyers, M.A., Mishra, A.Benson, D.J.: Mechanical properties of nanocrystalline materials. Prog. Mater. Sci. 51, 427 2006CrossRefGoogle Scholar