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Directional recrystallization and microstructures of an Fe–6.5wt%Si alloy

Published online by Cambridge University Press:  31 January 2011

Zhongwu Zhang
Affiliation:
Engineering Research Center of Materials Behavior and Design, Ministry of Education, Nanjing University of Science and Technology, Nanjing 210094, People’s Republic of China
Guang Chen*
Affiliation:
Engineering Research Center of Materials Behavior and Design, Ministry of Education, Nanjing University of Science and Technology, Nanjing 210094, People’s Republic of China; and Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
Hongbin Bei*
Affiliation:
Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831
Feng Li
Affiliation:
Engineering Research Center of Materials Behavior and Design, Ministry of Education, Nanjing University of Science and Technology, Nanjing 210094, People’s Republic of China
Feng Ye
Affiliation:
State Key Laboratory for Advanced Metals and Materials, USTB, Beijing 100083, People’s Republic of China
G.L. Chen
Affiliation:
Engineering Research Center of Materials Behavior and Design, Ministry of Education, Nanjing University of Science and Technology, Nanjing 210094, People’s Republic of China; and State Key Laboratory for Advanced Metals and Materials, USTB, Beijing 100083, People’s Republic of China
C.T. Liu
Affiliation:
Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831; and Mechanical Engineering Department, Hong Kong Polytechnic University, Hong Kong
*
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Abstract

Directional recrystallization of an Fe–6.5wt%Si alloy was investigated by changing hot zone temperatures and growth rates. Elongated (columnar) grains with an aspect ratio more than 10 can be produced when growth parameters are carefully adjusted. It was found that at a fixed growth rate, the grain length and aspect ratio increase with increased hot zone temperatures. At a fixed hot zone temperature, there is a critical growth rate at which columnar grains have the largest average aspect ratio. Below or above this growth rate, the aspect ratio decreases. Texture and grain orientation analysis showed that the preferentially selective growth to form columnar grains was favored by the formation of low-energy surfaces and grain boundaries.

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Articles
Copyright
Copyright © Materials Research Society 2009

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References

1Cairns, R.L., Curwick, L.R., and Benjamin, J.S.: Grain growth in dispersion strengthened superalloys by moving zone heat treatments. Metall. Trans. A 6, 179 (1975).CrossRefGoogle Scholar
2Duhl, D.N. and Thompson, E.R.: Directional structures for advanced aircraft turbine blades. J. Aircraft 14, 521 (1977).CrossRefGoogle Scholar
3Baloch, M.M. and Bhadeshia, H.K.D.H.: Directional recrystallization in Inconel MA 6000 nickel base oxide dispersion strengthened superalloy. Mater. Sci. Technol. 6, 1236 (1990).CrossRefGoogle Scholar
4Marsh, J.M. and Martin, J.W.: Micromechanisms of texture development during zone annealing of MA 6000 extrusions. Mater. Sci. Technol. 7, 183 (1991).CrossRefGoogle Scholar
5Humphreys, A.O., Shaw, S.W.K., and Martin, J.W.: Effect of process variables on the structure of directionally recrystallized MA-6000. Mater. Charact. 34, 9 (1995).CrossRefGoogle Scholar
6Greaves, M.S., Bate, P.S., Roberts, W.T., and Shaw, S.W.K.: Directional recrystallization in nickel based high temperature alloy. Mater. Sci. Technol. 12, 730 (1996).CrossRefGoogle Scholar
7Chou, T.S. and Bhadeshia, H.K.D.H.: Recrystallization temperatures in mechanically alloyed oxide-dispersion-strengthened MA956 and MA957 steels. Mater. Sci. Eng., A 189, 229 (1994).CrossRefGoogle Scholar
8Bhadeshia, H.K.D.H.: Recrystallization of practical mechanically alloyed iron-base and nickel-base superalloys. Mater. Sci. Eng., A 223, 64 (1997).CrossRefGoogle Scholar
9Baker, I., Iliescu, B., Li, J., and Frost, H.J.: Experiments and simulations of directionally annealed ODS MA 754. Mater. Sci. Eng., A 492, 353 (2008).CrossRefGoogle Scholar
10Baker, I. and Li, J.: Directional annealing of cold-rolled copper single crystals. Acta Mater. 50, 805 (2002).CrossRefGoogle Scholar
11Li, J., Johns, S.L., Iliescu, B.M., Frost, H.J., and Baker, I.: The effect of hot zone velocity and temperature gradient on the directional recrystallization of polycrystalline nickel. Acta Mater. 50, 4491 (2002).CrossRefGoogle Scholar
12Li, J. and Baker, I.: An EBSP study of directionally recrystallized cold-rolled nickel. Mater. Sci. Eng., A 392, 8 (2005).CrossRefGoogle Scholar
13Zhang, Z.W., Chen, G.L., and Chen, G.: The effect of drawing velocity and phase transformation on the structure of directionally annealed iron. Mater. Sci. Eng., A 434, 58 (2006).CrossRefGoogle Scholar
14Zhang, Z.W., Chen, G.L., and Chen, G.: Microstructural evolution of commercial pure iron during directional annealing. Mater. Sci. Eng., A 422, 241 (2006).CrossRefGoogle Scholar
15Zhang, Z.W., Chen, G.L., and Chen, G.: The effect of crystallographic texture on columnar grain growth in commercial pure iron during directional annealing. Mater. Sci. Eng., A 435–436, 573 (2006).CrossRefGoogle Scholar
16Zhang, Z.W., Chen, G.L., and Chen, G.: Dynamics and mechanism of columnar grain growth of pure iron under directional annealing. Acta Mater. 55, 5988 (2007).CrossRefGoogle Scholar
17Hirano, T., Mawari, T., Demura, M., and Isoda, Y.: Effect of direc-tional growth-rate on the mechanical properties of Ni3Al.Mater. Sci. Eng., A 239–240, 324 (1997).CrossRefGoogle Scholar
18Tsujimoto, T., Matsui, T., Suzuki, T., Tomota, Y., Shibue, K., and Furuyama, T.: Evolution of high aspect ratio grains in a TiAl-based alloy by directional grain growth. Intermetallics 9, 97 (2001).CrossRefGoogle Scholar
19Zhang, Z.W., Chen, G., Bei, H., Ye, F., Chen, G.L., and Liu, C.T.: Improvement of magnetic properties of an Fe–6.5 wt% Si alloy by directional recrystallization. Appl. Phys. Lett. 93, 191908 (2008).CrossRefGoogle Scholar
20Kim, K.N., Pan, L.M., Lin, J.P., Wang, Y.L., Lin, Z., and Chen, G.L.: The effect of boron content on the processing for Fe–6.5 wt% Si electrical steel sheets. J. Magn. Magn. Mater. 277, 331 (2004).CrossRefGoogle Scholar
21Ranganathan, S.: On the geometry of coincidence-site lattices. Acta Crystallogr. 21, 197 (1966).CrossRefGoogle Scholar
22Holm, E.A, Zacharoroulos, N., and Srolovitz, D.J.: Nonuniform and directional grain growth caused by grain boundary mobility variations. Acta Mater. 46, 953 (1998).CrossRefGoogle Scholar
23Arai, K.I., Tsutsumitake, H., and Ohmori, K.: Grain growth of rapid quenching high silicon-iron alloys. IEEE Trans. Magn. 20, p1463 (1984).CrossRefGoogle Scholar
24Arai, K.I. and Ohmori, K.: Grain growth characteristics and magnetic properties of rapidly quenched silicon steel ribbouns. Metall. Trans. A 17, 1295 (1986).CrossRefGoogle Scholar
25Watanabe, T., Fujii, H., Oikawa, H., and Arai, K.I.: Grain boundaries in rapidly solidified and annealed Fe–6.5mass%Si polycrys-talline ribbons with high ductility. Acta Metall. 37, 941 (1989).CrossRefGoogle Scholar
26Watanabe, T.: The importance of grain boundary character distribution (GBCD) to recrystallization, grain growth and texture. Scr. Metall. 27, 1479 (1992).Google Scholar