Hostname: page-component-cd9895bd7-mkpzs Total loading time: 0 Render date: 2024-12-28T16:25:30.907Z Has data issue: false hasContentIssue false

Effects of processing variables on microstructure formation in AZ31 magnesium alloys solidified with an electromagnetic vibration technique

Published online by Cambridge University Press:  31 January 2011

Mingjun Li*
Affiliation:
National Institute of Advanced Industrial Science and Technology, Materials Research Institute for Sustainable Development, Nagoya 463-8560, Japan
Takuya Tamura
Affiliation:
National Institute of Advanced Industrial Science and Technology, Materials Research Institute for Sustainable Development, Nagoya 463-8560, Japan
Kenji Miwa
Affiliation:
National Institute of Advanced Industrial Science and Technology, Materials Research Institute for Sustainable Development, Nagoya 463-8560, Japan
*
a)Address all correspondence to this author. e-mail: li.mingjun@aist.go.jp
Get access

Abstract

In the present study, we solidified magnesium-based AZ31 alloys by an electromagnetic vibration technique in a superconducting magnetic field at a vibration frequency of 500 Hz. Two groups of processing variables were used to carry out experiments; one is that the electric current is set as 60 A so as to testify to the influence of magnetic flux density on microstructure development from 1 up to 10 T. The other is that the electric current increases from 10 up to 120 A in the static magnetic field of 10 T, from which the dependence of structure formation on electric current is revealed. It is found that with the increase of both magnetic flux density and the level of electric current, solidified structures experience a transition from coarse dendrites to equiaxed grains. The melt fluid induced by the vibration force during solidification may promote the dendrite to a fragment. Meanwhile, the solids can be driven to move out of the operating region of the solute redistribution boundary. These effects make it difficult to form a complete dendrite but a refined structure. Furthermore, the vibration force can result in the formation of deformation twins in the alloy that has a low critical stress for basal slip. Regarding the effect of the electric current on microstructure, heat (measured in joules) can be produced when a large electric current is imposed, which can ripen the microstructure and induce a nonuniform structure. The slow cooling rate also makes the number fraction of deformation twinning decrease due to a rapid migration rate of atoms at high temperatures.

Type
Articles
Copyright
Copyright © Materials Research Society 2007

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1StJohn, D.H., Qian, M., Easton, M.A., Cao, P.Hildebrand, Z.: Grain refinement of magnesium alloys. Metall. Mater. Trans. A 36A, 1669 2005CrossRefGoogle Scholar
2Greer, A.L., Bunn, A.M., Tronche, A., Evans, P.V.Bristow, D.J.: Modelling of inoculation of metallic melts: Application to grain refinement of aluminium by Al-Ti-B. Acta Mater. 48, 2823 2000CrossRefGoogle Scholar
3Quested, T.E.Greer, A.L.: The effect of the size distribution of inoculant particles on as-cast grain size in aluminium alloys. Acta Mater. 52, 3859 2004CrossRefGoogle Scholar
4Qian, M.Das, A.: Grain refinement of magnesium alloys by zirconium: Formation of equiaxed grains. Scripta Mater. 54, 881 2006CrossRefGoogle Scholar
5Lee, Y.C., Dahle, A.K.StJohn, D.H.: The role of solute in grain refinement of magnesium. Metall. Mater. Trans. A 31, 2895 2000CrossRefGoogle Scholar
6Vives, Ch.: Effects of forced electromagnetic vibrations during the solidification of aluminum alloys: Part 1. Solidification in the presence of crossed alternating electric fields and stationary magnetic fields. Metall. Mater. Trans. B 27, 445 1996CrossRefGoogle Scholar
7Vives, Ch.: Electromagnetic refining of aluminum alloys by the CREM Process: I. Working principle and metallurgical results. Metall. Trans. B 20, 623 1989CrossRefGoogle Scholar
8Vives, Ch.: Grain refinement in aluminum alloys by means of electromagnetic vibrations including cavitation phenomena. http://www.tms.org/pubs/journals/JOM/9802/Vives/Vives-9802.html.,Google Scholar
9Guo, S., Le, Q., Zhao, Z., Wang, Z.Cui, J.: Microstructural refinement of DC cast AZ80 Mg billets by low frequency electromagnetic vibration. Mater. Sci. Eng., A 404, 323 2005CrossRefGoogle Scholar
10Dong, J., Cui, J., Zeng, X.Ding, W.: Effect of low-frequency electromagnetic vibration on cast-ability, microstructure and segregation of large-scale DC ingots of a high-alloyed Al. Mater Trans. 46, 94 2005Google Scholar
11Tamura, T., Amiya, K., Rachmat, R.S., Mizutani, Y.Miwa, K.: Electromagnetic vibration process for producing bulk metallic glasses. Nat. Mater. 4, 289 2005CrossRefGoogle ScholarPubMed
12Radjai, A., Miwa, K.Nishino, T.: An investigation of the effects caused by electromagnetic vibrations in a hypereutectic Al-Si alloy melt. Metall. Mater. Trans. A 29, 1477 1998CrossRefGoogle Scholar
13Radjai, A.Miwa, K.: Effects of the intensity and frequency of electromagnetic vibrations on the microstructural refinement of hypoeutectic Al-Si alloys. Metall. Mater. Trans. A 31, 755 2000CrossRefGoogle Scholar
14Radjai, A.Miwa, K.: Structural refinement of grey iron by electromagnetic vibrations. Metall. Mater. Trans. A 33, 3025 2002CrossRefGoogle Scholar
15Mizutani, Y., Kawai, S., Miwa, K., Yasue, K., Tamura, T.Sakaguchi, Y.: Effect of intensity and frequency of electromagnetic vibrations on refinement of primary silicon in Al-17% Si alloy. Mater. Trans. 45, 1939 2004CrossRefGoogle Scholar
16Mizutani, Y., Ohura, Y., Miwa, K., Yasue, K., Tamura, T.Sakaguchi, Y.: Effect of electromagnetic vibration intensity on microstructural refinement of Al-7% Si alloy. Mater. Trans. 45, 1944 2004CrossRefGoogle Scholar
17Mizutani, Y., Kawata, J., Miwa, K., Yasue, K., Tamura, T.Sakaguchi, Y.: Effect of frequency of electromagnetic vibrations on microstructural refinement of AZ91D magnesium alloy. J. Mater. Res. 19, 2997 2004CrossRefGoogle Scholar
18Mizutani, Y., Tamura, T.Miwa, K.: Microstructural refinement process of pure magnesium by electromagnetic vibrations. Mater. Sci. Eng., A 413-414, 205 2005CrossRefGoogle Scholar
19Mizutani, Y., Miwa, K., Tamura, T., Nakai, Y.Otsuka, Y.: Grain refinement of tough pitch copper by electromagnetic vibrations during solidification. Mater. Trans. 47, 1793 2006CrossRefGoogle Scholar
20Mizutani, Y., Tamura, T.Miwa, K.: Effect of electromagnetic vibration frequency and temperature gradient on grain refinement of pure aluminum. Mater. Trans. 48, 538 2007CrossRefGoogle Scholar
21Li, M., Tamura, T.Miwa, K.: Controlling microstructures of AZ31 magnesium alloys by an electromagnetic vibration technique during solidification: From experimental observation to theoretical understanding. Acta Mater. 55, 4635 2007CrossRefGoogle Scholar
22Hidemann, E.A.: Metallurgical effects of ultrasonic waves. J. Acoustic Soc. Am. 26, 831 1954CrossRefGoogle Scholar
23Avedesian, M.M.Baker, H.: Metallurgy and alloys in ASM Specialty Handbook Magnesium And Magnesium Alloys Materials International Society Materials Park, OH 1999 9, 15Google Scholar
24Davis, J.R.: Properties of pure aluminum in ASM Specialty Handbook Aluminum and Aluminum Alloys The Materials International Society Materials Park, OH 1993 641Google Scholar
25Li, M., Ishikawa, T., Nagashio, K., Kuribayashi, K.Yoda, S.: A comparative EBSP study of microstructure and microtexture formation from undercooled Ni99B1 melts solidified on an electrostatic levitator and an electromagnetic levitator. Acta Mater. 54, 3791 2006CrossRefGoogle Scholar
26Reed-Hill, R.E.Robertson, W.D.: Additional modes of deformation twinning in magnesium. Acta Metall. 5, 717 1957CrossRefGoogle Scholar
27Wang, Y.N.Huang, J.C.: The role of twinning and untwinning in yielding behavior in hot-extruded Mg–Al–Zn alloy. Acta Mater. 55, 897 2007CrossRefGoogle Scholar
28Hellawell, A., Sarazin, J.R.Steube, R.S.: Channel convection in partly solidified systems. Philos. Trans. R. Soc. London, Ser. A 345, 507 1993Google Scholar
29Flemings, M.C.: Behavior of metal alloys in the semisolid state. Metall. Trans. A 22, 957 1991CrossRefGoogle Scholar
30Kurz, W.Fisher, D.J.: Solute redistribution in Fundamentals of Solidification 3rd ed.Trans Tech Publications Ltd. Aedermannsdorf, Switzerland 1992 Chap. 6 117Google Scholar
31Marsh, S.P.Glicksman, M.E.: Overview of geometric effects on coarsening of mushy zones. Metall. Mater. Trans. A 27, 557 1996CrossRefGoogle Scholar
32Christian, J.W.Mahajan, S.: Deformation twinning. Prog. Mater. Sci. 39, 1 1995CrossRefGoogle Scholar
33Barnett, M.R., Keshavarz, Z.Nave, M.D.: Microstructural features of rolled Mg-3Al-1Zn. Metall. Mater. Trans. A 36, 1697 2005CrossRefGoogle Scholar