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Efficient visible light degradation of dyes in wastewater by nickel–phosphorus plating–titanium dioxide complex electroless plating fabric

Published online by Cambridge University Press:  07 February 2019

Xiaodong Ding ,
Wei Wang ,
Ao Zhang ,
Lishan Zhang  and
Dan Yu Open the ORCID record for Dan Yu [Opens in a new window]
Xiaodong Ding
Affiliation:
College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, Shanghai 201620, China; and Key Laboratory of Clean Dyeing and Finishing Technology of Zhejiang Province, Shaoxing University, Shaoxing 312000, China
Wei Wang
Affiliation:
College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, Shanghai 201620, China
Ao Zhang
Affiliation:
College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, Shanghai 201620, China
Lishan Zhang
Affiliation:
College of Resources and Environmental Science, Guangxi Normal University, Guilin, Guangxi 541004, China
Dan Yu*
Affiliation:
College of Chemistry, Chemical Engineering and Biotechnology, Donghua University, Shanghai 201620, China; and Key Laboratory of Clean Dyeing and Finishing Technology of Zhejiang Province, Shaoxing University, Shaoxing 312000, China
*
a)Address all correspondence to this author. e-mail: yudan@dhu.edu.cn
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Abstract

Dyeing wastewater has caused serious environmental problems nowadays. In this work, nickel–phosphorus plating–titanium dioxide (Ni-P-TiO2) electroless plating polyimide (PI) fabric was fabricated as an excellent visible light response composite. First, polyaniline (PANI) was in situ polymerized on the surface of the PI fabric. Second, PANI reduced palladium ions to be active seeds for initiating electroless plating of Ni-P-TiO2 layer. Finally, the Ni-P-TiO2/PANI/PI fabric with all-in-one structure was prepared, which can effectively overcome the drawbacks of poor loading fastness and insensitivity to visible light response. It was characterized by scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction, X-ray photoelectron spectroscopy, thermogravimetric analysis, and ultraviolet–visible diffuse reflectance spectroscopy. The photocatalytic activity was evaluated by degrading reactive blue 19, methylene blue, and reactive red (M-3BE) under visible light irradiation. The results show that the degradation rates of the all three dyes were over 91% with robust cycle stability for repeated 5 cycles of use. The possible photocatalytic degradation mechanism of fabrics was also proposed based on free radical and hole removal experiments.

Keywords

Ni-P-TiO2/PANI/PI fabricelectroless platingvisible lightphotocatalytic degradation
Type
Article
Information
Journal of Materials Research , Volume 34 , Issue 6 , 28 March 2019 , pp. 999 - 1010
Copyright
Copyright © Materials Research Society 2019 

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