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High temperature microcompression and nanoindentation in vacuum

Published online by Cambridge University Press:  14 September 2011

Sandra Korte ,
Robert J. Stearn ,
Jeffrey M. Wheeler  and
William J. Clegg
Sandra Korte*
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ, United Kingdom
Robert J. Stearn
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ, United Kingdom
Jeffrey M. Wheeler
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ, United Kingdom
William J. Clegg
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ, United Kingdom
*
a)Address all correspondence to this author. e-mail: Sandra.Korte@cantab.net
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Abstract

In small-scale testing at elevated temperatures, impurities in inert gases can pose problems so that testing in vacuum would be desirable. However, previous experiments have indicated difficulties with thermal stability and instrument noise. To investigate this, measurements of the temperature changes in a modified nanoindenter have been made and their influence on the displacement and load measurements is discussed. It is shown that controlling the temperatures of the indenter tip and the sample enabled flat punch indentations of gold, a good thermal conductor, to be carried out over several minutes at 665 °C in vacuum, as well as permitting thermal stability to be quickly re-established in site-specific microcompression experiments. This allowed compression of nickel superalloy micropillars up to sample temperatures of 630 °C with very low levels of oxidation after 48 h. Furthermore, the measured Young moduli, yield and flow stresses were consistent with literature data.

Keywords

NanoindentationAuStress/strain relationship
Type
Articles
Information
Journal of Materials Research , Volume 27 , Issue 1: Focus Issue: Instrumented Indentation , 14 January 2012 , pp. 167 - 176
Copyright
Copyright © Materials Research Society 2011

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