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Investigation on Structure Transition of Fullerene During Mechanical Alloying and Subsequent Treatments

Published online by Cambridge University Press:  31 January 2011

Z. G. Liu ,
H. Ohi ,
K. Masuyama ,
K. Tsuchiya  and
M. Umemoto
Z. G. Liu
Affiliation:
Department of Production Systems Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi 441–8580, Japan
H. Ohi
Affiliation:
Department of Production Systems Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi 441–8580, Japan
K. Masuyama
Affiliation:
Department of Mechanical Engineering, Toyama National College of Technology, 13 Hongoumachi, Toyama 939, Japan
K. Tsuchiya
Affiliation:
Department of Production Systems Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi 441–8580, Japan
M. Umemoto
Affiliation:
Department of Production Systems Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi 441–8580, Japan
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Abstract

Mechanical milling of fullerene (soot containing C60/C70 fullerenes in a 8:2 molar ratio) was investigated through various characterization methods. It was found that mechanical milling would not destroy the molecular structure of fullerene C60 (C70), while the long-range order of the face-centered-cubic crystalline structure was easily modified and transformed into amorphous phase, a mixture of fullerene C60 (C70) polymers and monomers. Differential scanning calorimetry analysis revealed a recovery of polymers to pristine fullerene molecules at 678 K, which is much higher than the reported depolymerization temperature of fullerene polymers induced by photo irradiation and by high-pressure–temperature processes. It is suggested that the contaminated Fe acts as a catalyst in the polymerization process.

Type
Articles
Information
Journal of Materials Research , Volume 15 , Issue 7 , July 2000 , pp. 1528 - 1537
Copyright
Copyright © Materials Research Society 2000

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References

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