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The microstructure and corrosion resistance of biological Mg–Zn–Ca alloy processed by high-pressure torsion and subsequently annealing

Published online by Cambridge University Press:  14 March 2017

Congzheng Zhang ,
Shaokang Guan ,
Liguo Wang ,
Shijie Zhu  and
Lei Chang
Congzheng Zhang
Affiliation:
School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, People’s Republic of China
Shaokang Guan*
Affiliation:
School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, People’s Republic of China
Liguo Wang
Affiliation:
School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, People’s Republic of China
Shijie Zhu
Affiliation:
School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, People’s Republic of China
Lei Chang
Affiliation:
School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, People’s Republic of China
*
a) Address all correspondence to this author. e-mail: skguan@zzu.edu.cn
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Abstract

Magnesium alloy has great potential for bone implantation. However, its corrosion rate is fast in physiological environment. In this paper, biological Mg–Zn–Ca alloy was processed by high pressure torsion (HPT) and subsequently annealed at 90–270 °C for 30 min. The microstructure and corrosion resistance in simulated body fluid were investigated. The results revealed that with the rise of the annealing temperature, the grain size of the HPT alloy gradually increased and the relative diffraction peak intensity of (0002) grain orientation decreased. The amount of second phases increased first and then decreased, while the surface stress decreased first and then increased. All of these changes affected the corrosion rate simultaneously. The corrosion resistance of the HPT alloy increased first and then decreased with the rise of annealing temperature. After annealing at 210 °C for 30 min, the corrosion resistance was the best. Therefore, it was feasible to control the corrosion rate via annealing treatment.

Keywords

Mgmicrostructurecorrosion
Type
Articles
Information
Journal of Materials Research , Volume 32 , Issue 6 , 28 March 2017 , pp. 1061 - 1072
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Copyright
Copyright © Materials Research Society 2017 

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Footnotes

Contributing Editor: Jürgen Eckert

References

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