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Microstructures and material properties of fibrous Al2O3–(m-ZrO2)/t-ZrO2 composites fabricated by a fibrous monolithic process

Published online by Cambridge University Press:  01 November 2004

Byong-Taek Lee*
Affiliation:
School of Advanced Materials Engineering, Kongju National University, Kongju City, Chungnam 314-701, Korea
Ki-Hyun Kim
Affiliation:
School of Advanced Materials Engineering, Kongju National University, Kongju City, Chungnam 314-701, Korea
Jae-Kil Han
Affiliation:
School of Advanced Materials Engineering, Kongju National University, Kongju City, Chungnam 314-701, Korea
*
a) Address all correspondence to this author. e-mail: lbt@kongju.ac.kr
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Abstract

Al2O3–(m-ZrO2)/t-ZrO2 composite having fibrous and homogeneous microstructure was successfully fabricated using a fibrous monolithic process. The composites had a homogeneous microstructure as well as good interfaces between the Al2O3–(m-ZrO2) and t-ZrO2 phases. The thickness of each phases were reduced to 375, 50, 5 μm, and 0.7 μm as the number of extrusion passes increased up to 5. The material properties of density, hardness, bending strength, and fracture toughness increased as the passes of extrusion were increased up to a fifth pass, and their maximum values were about 98.5%, 1230 Hv, 570 MPa, and 6.5 MPa⋅m1/2, respectively. The fracture toughnesses in the direction of longitudinal and transverse direction of the fifth passed sample showed the different values with about 6.5 and 5.4 MPa⋅m1/2, respectively.

Type
Articles
Copyright
Copyright © Materials Research Society 2004

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References

REFERENCES

1Farmer, C. and Sayir, A.: Tensile strength and microstructure of Al2O3–ZrO2 hypo-eutectic fibers. Eng. Fract. Mech. 69, 1015 (2002).CrossRefGoogle Scholar
2Tarlazzi, E., Roncari, E., Pinasco, P., Guicciardi, S., Melandri, C. and de Portu, G.: Tribological behaviour of Al2O3/ZrO2-ZrO2 laminated composites. Wear 29, 244 (2000).Google Scholar
3Jrdan, D.R.: Anophthalmic orbital implants. Ophthalmol. Clin. North Am. 13, 587 (2000).CrossRefGoogle Scholar
4Fruh, H.J., Willmann, G. and Pfaff, H.G.: Wear characteristics of ceramic-on-ceramic for hip endoprostheses. Biomaterials 18, 873 (1997).CrossRefGoogle ScholarPubMed
5Evans, G. and Heuer, A.H.: Transforemation toughness in ceramics martensite transformations in crack-tip stress fields. J. Am. Ceram. Soc. 63, 5 (1980).CrossRefGoogle Scholar
6Lee, B.T., Lee, K.H. and Hiraga, K.: Stress-induced phase transformation of ZrO2 in ZrO2(3-mol% Y2O3)-25 vol% Al2O3 composite studied by transmission electron microscopy. Scripta Mater. 38, 1101 (1998).CrossRefGoogle Scholar
7Lee, B.T. and Hiraga, K.: Crack propagation and deformation behavior of Al2O3-24 vol% ZrO2 composite studied by transmission electron microscopy. J. Mater. Res. 9, 1199 (1994).CrossRefGoogle Scholar
8Lee, B.T., Nishiyama, A. and Hiraga, K.: Micro-indentation fracture behavior of Al2O3-24 vol% ZrO2(Y2O3) composites studied by transmission electron microscopy. Mater. Trans., JIM 34, 682 (1993).CrossRefGoogle Scholar
9Claussen, N., Steeb, J. and Pabst, R.F.: Effect of induced microcracking on the fracture toughness of ceramics. Ceram. Bull. 56, 559 (1977).Google Scholar
10Lee, B.T., Hiraga, K., Shindo, D. and Nishiyama, A.: Microstructure of pressureless-sintered Al2O3-24 vol% ZrO2 composite studied by high-resolution electron microscopy. J. Mater. Sci. 29, 959 (1994).CrossRefGoogle Scholar
11Strum, A., Betz, U., Scipione, G. and Hahn, H.: Grain growth and phase stability in a nanocrystalline ZrO2-15 wt% Al2O3 ceramic. Nanostruct. Mater. 11, 651 (1999).CrossRefGoogle Scholar
12Celli, A., Tucci, A., Esposito, L. and Palmonari, C.: Fractal analysis of cracks in alumina–zirconia composites. J. Eur. Ceram. Soc. 23, 469 (2003).CrossRefGoogle Scholar
13Betz, U., Sturm, A., Lofflor, J.F., Wagner, W., Wiedenmann, A. and Hahn, H.: Microstructural development during final-stage sintering of nanostructured zirconia based ceramics. Mater. Sci. Eng. A 281, 68 (2000).CrossRefGoogle Scholar
14Miyazaki, H., Yoshizawa, Y. and Hirao, K.: Preparation and mechanical properties of 10 vol% zirconia/alumina composite with fine-scale fibrous microstructure by co-extrusion process. Mater. Lett. 58, 1410 (2004).CrossRefGoogle Scholar
15Kaya, C., Butler, E.G. and Lewis, M.H.: Co-extursion of Al2O3/ZrO2 bi-phase high temperature ceramics with fine scale aligned microstructure. Eur. Ceram. Soc. 23, 935 (2003).CrossRefGoogle Scholar
16Kim, T.S., Kim, K.H., Goto, T. and Lee, B.T.: Microsturcture control of Al2O3/ZrO2 composite by fibrous monolithic process. Mater. Trans., JIM 45, 1 (2004).CrossRefGoogle Scholar
17Garvie, R.C., Hannink, R.H.J. and Swain, M.V.: X-ray analysis of the transformed zone in partially stabilized zirconia (PSZ). J. Mater. Sci. Lett. 1, 437 (1982).CrossRefGoogle Scholar