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Nanoindentation-induced deformation, microfracture, and phase transformation in crystalline materials investigated in situ by acoustic emission

Published online by Cambridge University Press:  17 February 2020

Xiao-Guang Ma  and
Kyriakos Komvopoulos Open the ORCID record for Kyriakos Komvopoulos [Opens in a new window]
Xiao-Guang Ma
Affiliation:
Department of Mechanical Engineering, University of California, Berkeley, California 94720, USA
Kyriakos Komvopoulos*
Affiliation:
Department of Mechanical Engineering, University of California, Berkeley, California 94720, USA
*
a)Address all correspondence to this author. e-mail: kyriakos@me.berkeley.edu
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Abstract

With the ever-increasing importance of nanoscale deformation phenomena in contemporary technologies, basic understanding of material behavior at the nanoscale has become of critical importance. Especially, nanomechanical testing that provides the capability to study fundamental nanoscale deformation and phase change phenomena in real time and under controlled loading conditions is essential for nanomaterial research. In this study, acoustic emission (AE) was used in situ to characterize nanoindentation-induced deformation, microfracture, and phase transformation processes intrinsic of bulk single-crystal MgO and polycrystalline Al, thin films of polycrystalline SiC, and thick films of austenitic TiNi shape-memory alloy. Scale-dependent plastic deformation and microfracture affected by the indenter tip radius and the applied normal load are interpreted in terms of the type and intensity of AE events revealed by abrupt displacement excursions in the loading response of the indented materials. The amplitudes of AE waveforms are used to examine characteristic deformation, microfracture, and phase change mechanisms in the time domain. Fast Fourier transformation and short-time Fourier transformation analyses provide further insight into the material behavior and structural changes due to indentation loading in the frequency and time-frequency domain, respectively. The methodology developed in this study represents an effective approach for nanomechanical testing and in situ characterization of nanoscale deformation, microfracture, and phase transformation phenomena.

Keywords

acoustic emissiondislocationsdisplacement excursionmicrofracturenanoindentationphase transformationplastic deformation
Type
Article
Information
Journal of Materials Research , Volume 35 , Issue 4 , 28 February 2020 , pp. 380 - 390
Copyright
Copyright © Materials Research Society 2020

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Footnotes

b)

Present address: International Institute for Urban Systems Engineering, Southeast University, Nanjing 210096, China.

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