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A novel method for synthesis of carbon nanotubes: Low temperature solid pyrolysis

Published online by Cambridge University Press:  31 January 2011

Y. L. Li
Affiliation:
Department of Micro-Crystalline & Laser Processing, Chinese Academy of Sciences, 72 Wenhua Road, Shenyang 110015, China
Y. D. Yu
Affiliation:
Laboratory of Atomic Imaging of Solids, Institute of Metal Research, Chinese Academy of Sciences, 72 Wenhua Road, Shenyang 110015, China
Y. Liang
Affiliation:
Department of Micro-Crystalline & Laser Processing, Chinese Academy of Sciences, 72 Wenhua Road, Shenyang 110015, China
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Abstract

We report a novel method for the synthesis of carbon nanotubes: low temperature solid pyrolysis. By pyrolysis of hexamethyldisilazane-derived silicon carbonitride powders in a graphite furnace, we synthesized carbon nanotubes at 1400 °C. This new method has advantages of in situ growth of the carbon nanotubes, is stable in the synthesis process, and is technically simpler than conventional arc-discharge methods.

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Articles
Copyright
Copyright © Materials Research Society 1997

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References

REFERENCES

1.Iijima, S., Nature (London) 354, 56 (1992).CrossRefGoogle Scholar
2.Iijima, S., MRS Bull., November, 43 (1994).CrossRefGoogle Scholar
3.Ajayan, P. M. and Iijima, S., Nature (London) 361, 333 (1993).CrossRefGoogle Scholar
4.Tersoff, J. and Ruoff, R. S., Phys. Rev. Lett. 73, 676 (1994).CrossRefGoogle Scholar
5.Ebbesen, T. W. and Ajayan, P. M., Nature (London) 358, 220 (1992).CrossRefGoogle Scholar
6.Iijima, S. and Ichihashi, T., Nature (London) 363, 603 (1993).CrossRefGoogle Scholar
7.Saito, T., Yoshikawa, T., Inagaki, M., Tomita, M., and Hayashi, T., Chem. Phys. Lett. 204, 2774 (1992).Google Scholar
8.Colbert, D. T., Zhang, J., McClure, S. M., Nilolaev, P., Chen, Z., Hafner, J. H., Owens, D. W., Kotula, P. G., Carter, C. B., Weaver, J. H., Rinzler, A. G., and Smalley, R. E., Science 266, 1218 (1994).CrossRefGoogle Scholar
9.Lin, X., Wang, X. K., Dravid, V. P., Chang, R. P. H., and Ketterson, J. B., Appl. Phys. Lett. 64, 181 (1994).CrossRefGoogle Scholar
10.Wang, X. K., Lin, X. W., Dravid, V. P., Ketterson, J. B., and Chang, R. P. H., Appl. Phys. Lett. 66, 2430 (1995).CrossRefGoogle Scholar
11.Zhoa, D., Seraphin, S., and Wang, S., Appl. Phys. Lett. 65, 1593 (1994).CrossRefGoogle Scholar
12.Seraphin, S. and Zhou, D., Appl. Phys. Lett. 64, 2087 (1994).CrossRefGoogle Scholar
13.Ivanov, V., Nagy, J. B., Lambin, Ph., Lucas, A., Zhang, X. B., Zhang, X. F., Bernaerts, D., Van Tendeloo, G., Amelinckx, S., and Landuyt, J. V., Chem. Phys. Lett. 223, 329 (1994).CrossRefGoogle Scholar
14.Hatta, N. and Murata, K., Chem. Phys. Lett. 217, 398 (1994).CrossRefGoogle Scholar
15.Jose-Yacaman, M., Terrones, H., and Rendon, L., Carbon 33, 669 (1995).CrossRefGoogle Scholar
16.Iijima, S., Ichihashi, T., and Ando, Y., Nature (London) 356, 776 (1992).Google Scholar
17.Iijima, S., Ajayan, P. M., and Ichihashi, T., Phys. Rev. Lett. 69, 3100 (1992).CrossRefGoogle Scholar
18.Wang, M. J. and Wada, H. J., J. Mater. Sci. 25, 1690 (1990).CrossRefGoogle Scholar
19.Campbell, W. B., in Whisker Technology, edited by Levitt, A. P. (John Wiley & Sons, New York, 1970), p. 15.Google Scholar
20.Ramesh, P. D. and Rao, K. J., J. Mater. Res. 9, 2330 (1994).CrossRefGoogle Scholar
21.Li, Y. L., Liang, Y., and Hu, Z. Q., Ceram. Int. 21, 59 (1994).CrossRefGoogle Scholar
22.Li, Y. L., Liang, Y., Xiao, K. S., Zheng, F., and Hu, Z. Q., Mater. Lett. 22, 87 (1995).CrossRefGoogle Scholar
23.Rice, G. W. and Woodin, R. L., J. Mater. Res. 4, 1538 (1989).CrossRefGoogle Scholar
24.Li, Y. L., Liang, Y., and Hu, Z. Q., Nano. Mater. 4, 857 (1994).CrossRefGoogle Scholar
25.Rice, G. W., J. Am. Ceram. Soc. 69, C183 (1986).CrossRefGoogle Scholar