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On the role of vibration frequency on the solidification of AZ91D magnesium alloys during electromagnetic vibration

Published online by Cambridge University Press:  31 January 2011

Mingjun Li*
Affiliation:
National Institute of Advanced Industrial Science and Technology, Materials Research Institute for Sustainable Development, Nagoya 463-8560, Japan
Takuya Tamura
Affiliation:
National Institute of Advanced Industrial Science and Technology, Materials Research Institute for Sustainable Development, Nagoya 463-8560, Japan
Kenji Miwa
Affiliation:
National Institute of Advanced Industrial Science and Technology, Materials Research Institute for Sustainable Development, Nagoya 463-8560, Japan
*
a) Address all correspondence to this author. e-mail: li.mingjun@aist.go.jp
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Abstract

In the present paper, we solidified magnesium-based AZ91D alloys in a superconducting magnetic field when an alternating current flowed through the alloy. As the direction of the magnetic field is perpendicular to that of the alternating current, a periodic electromagnetic force is produced to activate an electromagnetic vibration (EMV) on the alloy during solidification. The microstructure formation and microtexture evolution processed by EMV were examined. A significant difference arises in electrical resistivity between a solid and a liquid in the mushy zone of the alloy, making the solid move faster than the liquid and thus generating uncoupled motion, from which melt flow is initiated. The texture evolution obtained by x-ray diffraction and electron backscatter diffraction (EBSD) mapping reveal a strong dependence of melt flow intensity versus vibration frequency. A further analysis reveals that melt flow is rather weak when the vibration frequency is too low and thus the segmentation of growing crystals cannot be thoroughly completed. At medium vibration frequencies, severe fluid flow occurs, which favors fragmentation and thus results in a refined microstructure and a random microtexture. When the vibration frequency is too high, the relative leading distance covered by the mobile solid is rather short and melt flow once again becomes weak. Meanwhile, the static magnetic field makes the crystals orient to their easy magnetization direction and thus yields highly aligned textures. Experimentally, the present systematic observation indicates that the role of melt flow is of substantial importance in revealing the origin of structure formation when the alloy is solidified at various vibration frequencies.

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Articles
Copyright
Copyright © Materials Research Society 2009

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References

REFERENCES

1.StJohn, D.H., Qian, M., Easton, M.A., Cao, P., Hildebrand, Z.: Grain refinement of magnesium alloys. Metall. Mater. Trans. A 36, 1669 2005CrossRefGoogle Scholar
2.Greer, A.L., Bunn, A.M., Tronche, A., Evans, P.V., Bristow, D.J.: Modelling of inoculation of metallic melts: Application to grain refinement of aluminium by Al-Ti-B. Acta Mater. 48, 2823 2000CrossRefGoogle Scholar
3.Quested, T.E., Greer, A.L.: The effect of the size distribution of inoculant particles on as-cast grain size in aluminum alloys. Acta Mater. 52, 3859 2004CrossRefGoogle Scholar
4.Flemings, M.C.: Behavior of metal alloys in the semisolid state. Metall. Trans. A 22, 957 1991CrossRefGoogle Scholar
5.Fan, Z.: Semisolid metal processing. Int. Mater. Rev. 47, 49 2002CrossRefGoogle Scholar
6.Fan, Z., Liu, G., Wang, Y.: Microstructure and mechanical properties of rheo-diecast AZ91D magnesium alloy. J. Mater. Sci. 41, 3631 2006CrossRefGoogle Scholar
7.Fan, Z., Liu, G.: Solidification behavior of AZ91D alloy under intensive forced convection in the RDC process. Acta Mater. 53, 4345 2005CrossRefGoogle Scholar
8.Vives, Ch.: Effects of forced electromagnetic vibrations during the solidification of aluminum alloys: Part 1. Solidification in the presence of crossed alternating electric fields and stationary magnetic fields. Metall. Mater. Trans. B 27, 445 1996CrossRefGoogle Scholar
9.Vives, C.: Electromagnetic refining of aluminum alloys by the CREM process. I. Working principle and metallurgical results. Metall. Mater. Trans. B 20, 623 1989CrossRefGoogle Scholar
10.Vives, C.: Grain refinement in aluminum alloys by means of electromagnetic vibrations including cavitation phenomena. JOM-e 1998 50http://www.tms.org/pubs/journals/JOM/9802/Vives/Vives-9802.html.Google Scholar
11.Dong, J., Cui, J., Yu, F., Ban, C., Zhao, Z.: Effect of low-frequency electromagnetic casting on the castability, microstructure, and tensile properties of direct-chill cast Al-Zn-Mg-Cu alloy. Metall. Mater. Trans. A 35, 2487 2004CrossRefGoogle Scholar
12.Guo, S., Le, Q., Zhao, Z., Wang, Z., Cui, J.: Microstructural refinement of DC cast AZ80 Mg billets by low frequency electromagnetic vibration. Mater. Sci. Eng., A 404, 323 2005CrossRefGoogle Scholar
13.Radjai, A., Miwa, K., Nishino, T.: An investigation of the effects caused by electromagnetic vibrations in a hypereutectic Al-Si alloy melt. Metall. Mater. Trans. A 29, 1477 1998CrossRefGoogle Scholar
14.Radjai, A., Miwa, K.: Effects of the intensity and frequency of electromagnetic vibrations on the microstructural refinement of hypoeutectic Al-Si alloys. Metall. Mater. Trans. A 31, 755 2000CrossRefGoogle Scholar
15.Radjai, A., Miwa, K.: Structural refinement of gray iron by electromagnetic vibrations. Metall. Mater. Trans. A 33, 3025 2002CrossRefGoogle Scholar
16.Mizutani, Y., Kawai, S., Miwa, K., Yasue, K., Tamura, T., Sakaguchi, Y.: Effect of intensity and frequency of electromagnetic vibrations on refinement of primary silicon in Al-17% Si alloy. Mater. Trans. 45, 1939 2004CrossRefGoogle Scholar
17.Mizutani, Y., Ohura, Y., Miwa, K., Yasue, K., Tamura, T., Sakaguchi, Y.: Effect of electromagnetic vibration intensity on microstructural refinement of Al-7% Si alloy. Mater. Trans. 45, 1944 2004CrossRefGoogle Scholar
18.Mizutani, Y., Kawata, J., Miwa, K., Yasue, K., Tamura, T., Sakaguchi, Y.: Effect of frequency of electromagnetic vibrations on microstructural refinement of AZ91D magnesium alloy. J. Mater. Res. 19, 2997 2004CrossRefGoogle Scholar
19.Mizutani, Y., Tamura, T., Miwa, K.: Microstructural refinement process of pure magnesium by electromagnetic vibrations. Mater. Sci. Eng., A 413–414, 205 2005CrossRefGoogle Scholar
20.Mizutani, Y., Miwa, K., Tamura, T., Nakai, Y., Otsuka, Y.: Grain refinement of tough pitch copper by electromagnetic vibrations during solidification. Mater. Trans. 47, 1793 2006CrossRefGoogle Scholar
21.Mizutani, Y., Tamura, T., Miwa, K.: Effect of electromagnetic vibration frequency and temperature gradient on grain refinement of pure aluminum. Mater. Trans. 48, 538 2007CrossRefGoogle Scholar
22.Hidemann, E.A.: Metallurgical effects of ultrasonic waves. J. Acoust. Soc. Am. 26, 831 1954CrossRefGoogle Scholar
23.Abramov, O.V.: Action of high intensity ultrasound on solidifying metal. Ultrasonics 25, 73 1987CrossRefGoogle Scholar
24.Li, M., Tamura, T., Miwa, K.: Controlling microstructures of AZ31 magnesium alloys by an electromagnetic vibration technique during solidification: From experimental observation to theoretical understanding. Acta Mater. 55, 4635 2007CrossRefGoogle Scholar
25.Avedesian, M.M., Baker, H.: ASM Specialty Handbook Magnesium and Magnesium Alloys The Materials International Society Materials Park, OH 1999 915Google Scholar
26.Davis, J.R.: ASM Specialty Handbook Aluminum and Aluminum Alloys The Materials International Society Materials Park, OH 1993 641Google Scholar
27.Davis, S.T., Schulze, T.P.: Effects of flow on morphological stability during directional solidification. Metall. Mater. Trans. A 27, 583 1996CrossRefGoogle Scholar
28.Hansen, G.C., Hellawell, A., Lu, S.Z., Steube, R.S.: Some consequences of thermosolutal convection: The grain structure of castings. Metall. Mater. Trans. A 27, 569 1996CrossRefGoogle Scholar
29.Li, M., Ishikawa, T., Nagashio, K., Kuribayashi, K., Yoda, S.: A comparative EBSP study of microstructure and microtexture formation from undercooled Ni99B1 melts solidified on an electrostatic levitator and an electromagnetic levitator. Acta Mater. 54, 3791 2006CrossRefGoogle Scholar
30.Hellawell, A., Liu, S., Lu, S.Z.: Dendrite fragmentation and the effects of fluid flow in castings. JOM 54, 318 1997CrossRefGoogle Scholar
31.Asai, S.: Application of high magnetic fields in inorganic materials processing. Modell. Simul. Mater. Sci. Eng. 12, R1 2004CrossRefGoogle Scholar
32.Landolt-Bornstein, : Properties of Materials and Their Phases, 10 teil, Magnetic Properties II Springer-Verlag Berlin 1967 144Google Scholar
33.Wu, C., Li, S., Sassa, K., Chino, Y., Hattori, K., Asai, S.: The theoretical analysis of crystal alignment of feeble magnetic materials under high magnetic field. Mater. Trans. 46, 1311 2005CrossRefGoogle Scholar
34.Li, M., Tamura, T., Miwa, K.: Microstructure and microtexture formation of AZ91D magnesium alloys solidified in a static magnetic field. Metall. Mater. Trans. A (Submitted)Google Scholar
35.Martinez, R.A., Karma, A., Flemings, M.C.: Spheroidal particle stability in semisolid processing. Metall. Mater. Trans. A 37, 2807 2006CrossRefGoogle Scholar