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Pb(ZrxTi1−x)O3 ceramics via reactive sintering of partially reacted mixture produced by a high-energy ball milling process

Published online by Cambridge University Press:  31 January 2011

L. B. Kong ,
J. Ma ,
T. S. Zhang ,
W. Zhu  and
O. K. Tan
L. B. Kong
Affiliation:
School of Materials Engineering, Nanyang Technological University, Singapore 639798
J. Ma
Affiliation:
School of Materials Engineering, Nanyang Technological University, Singapore 639798
T. S. Zhang
Affiliation:
School of Materials Engineering, Nanyang Technological University, Singapore 639798
W. Zhu
Affiliation:
Microelectronics Center, School of Electric and Electronic Engineering, Nanyang Technological University, Singapore 639798
O. K. Tan
Affiliation:
Microelectronics Center, School of Electric and Electronic Engineering, Nanyang Technological University, Singapore 639798
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Abstract

Partially reacted mixtures of Pb(ZrxTi1−x)O3 and its corresponding starting oxide components were obtained by a high-energy ball milling process. The partially reacted powders were characterized by x-ray diffraction and scanning electron microscopy techniques. The sintering behavior of the milled mixtures has demonstrated a distinct volumetric expansion before the densification of the samples, which clearly shows the occurrence of a reactive sintering process of the partially reacted powders. Such process requires a lower densification temperature as compared with the PZT powders produced by the conventional solid-state reaction process. PZT ceramics were found to form directly from the partially reacted powders sintered at 900–1200 °C. The dielectric and ferroelectric properties of the PZT ceramics as a function of sintering temperature and milling time were also studied and discussed.

Type
Articles
Information
Journal of Materials Research , Volume 16 , Issue 6 , June 2001 , pp. 1636 - 1643
Copyright
Copyright © Materials Research Society 2001

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References

REFERENCES

1.Jaffe, B., Cook, W.R. Jr., and Jaffe, H., Piezoelectric Ceramics (Academic Press, New York, 1971).Google Scholar
2.Uchino, K., Piezoelectric Actuators and Ultrasonic Motors (Kluwer, Boston, MA, 1997).Google Scholar
3.Elissalde, G., Cross, L.E., and Randall, C.A., J. Am. Ceram. Soc. 79, 2041 (1996).CrossRefGoogle Scholar
4.Wang, Q.M. and Cross, L.E., J. Am. Ceram. Soc. 82, 103 (1999).CrossRefGoogle Scholar
5.Matsuo, Y. and Sasaki, H., J. Am. Ceram. Soc. 48, 289 (1965).CrossRefGoogle Scholar
6.Chandratreya, S.S., Fulrath, R.M., and Pask, J.A., J. Am. Ceram. Soc. 64, 422 (1981).CrossRefGoogle Scholar
7.Mishra, S.K., Singh, A.P., and Pandey, D., Philosoph. Mag. B 76, 213 (1997).CrossRefGoogle Scholar
8.Rao, K.R.M., Rao, A.V.P., and Komarneni, S., Mater. Lett. 28, 463 (1996).CrossRefGoogle Scholar
9.Hirashima, H., Onishi, E., and Nakagowa, M., J. Non-Cryst. Solids 121, 404 (1990).CrossRefGoogle Scholar
10.Kutty, T.R.N. and Balachandran, R., Mater. Res. Bull 19, 1479 (1984).CrossRefGoogle Scholar
11.Calka, A. and Radlinski, A.P., Mater. Sci. Eng A 134, 1350 (1991).CrossRefGoogle Scholar
12.Welham, N.J., Willis, P.E., and Kerr, T., J. Am. Ceram. Soc. 83, 33 (2000).CrossRefGoogle Scholar
13.Jiang, J.Z., Poulsen, F.W., and Mørup, S., J. Mater. Res. 14, 1343 (1999).CrossRefGoogle Scholar
14.Jiang, J.Z., Lin, R., Lin, W., Nielsen, K., Mørup, S., Dam-Johansen, K., and Clasen, R., J. Phys. D: Appl. Phys. 30, 1458 (1997).CrossRefGoogle Scholar
15.Simoneau, M., L’Esperance, G., Trudeau, J.L., and Schultz, R., J. Mater. Res. 9, 535 (1994).CrossRefGoogle Scholar
16.Fatemi, D.J., Harris, V.G., Browning, V.M., and Kirkland, J.P., J. Appl. Phys. 83, 6867 (1998).CrossRefGoogle Scholar
17.Xue, J., Wan, D., Lee, S.E., and Wang, J., J. Am. Ceram. Soc. 82, 1687 (1999).CrossRefGoogle Scholar
18.Kong, L.B., Zhu, W., and Tan, O.K., Mater. Lett. 42, 232 (2000).CrossRefGoogle Scholar
19.Wang, J., Wan, D., Xue, J., and Ng, W.B., J. Am. Ceram. Soc. 82, 477 (1999).CrossRefGoogle Scholar
20.Wan, D.M., Xue, J.M., and Wang, J., Acta Mater. 47, 2283 (1999).CrossRefGoogle Scholar
21.Shrout, T.R., Patet, P., Kim, S., and Lee, G.S., J. Am. Ceram. Soc. 73, 1862 (1990).CrossRefGoogle Scholar
22.Kong, L.B., Ma, J., Zhu, W., and Tan, O.K., Scripta. Mater. 44, 245 (2001).Google Scholar
23.Hammer, M. and Hoffmann, M.J., J. Am. Ceram. Soc. 81, 3277 (1998).CrossRefGoogle Scholar
24.Chen, H.D., Udayakumar, K.R., Gaskey, C.J., Cross, L.E., Bernstein, J.J., and Niles, L.C., J. Am. Ceram. Soc. 79, 2189 (1996).CrossRefGoogle Scholar
25.Randall, C.A., Kim, N., Kucera, J.P., Cao, W., and Shrout, T.R., J. Am. Ceram. Soc. 81, 677 (1998).CrossRefGoogle Scholar
26.Jovalekic, C., Zdujic, M., Radakovic, A., and Mitric, M., Mater. Lett. 24, 365 (1995).CrossRefGoogle Scholar