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Printing composite nanofilaments for use in a simple and low-cost 3D pen

Published online by Cambridge University Press:  20 April 2020

Francisca Pereira de Araujo
Affiliation:
LIMAV—Interdisciplinary Laboratory for Advanced Materials, UFPI—Federal University of Piaui, Teresina, Piauí 64049-550, Brazil
Igor Tadeu Silva Batista
Affiliation:
Research Center on Biotechnology—Uniara, Araraquara, São Paulo 14801-340, Brazil
Francílio Carvalho de Oliveira
Affiliation:
Universidade Estácio, Teresina, Piauí 64 046-700, Brazil
Layane Rodrigues de Almeida
Affiliation:
LIMAV—Interdisciplinary Laboratory for Advanced Materials, UFPI—Federal University of Piaui, Teresina, Piauí 64049-550, Brazil
Guilherme de Castro Brito
Affiliation:
Universidade Estácio, Teresina, Piauí 64 046-700, Brazil
Hernane da Silva Barud
Affiliation:
Research Center on Biotechnology—Uniara, Araraquara, São Paulo 14801-340, Brazil
Dalton Dittz
Affiliation:
Biochemistry and Pharmacology Department, Federal University of Piauí, Teresina, Piauí 64049-550, Brazil
Edson Cavalcanti Silva-Filho
Affiliation:
LIMAV—Interdisciplinary Laboratory for Advanced Materials, UFPI—Federal University of Piaui, Teresina, Piauí 64049-550, Brazil
Josy Anteveli Osajima*
Affiliation:
LIMAV—Interdisciplinary Laboratory for Advanced Materials, UFPI—Federal University of Piaui, Teresina, Piauí 64049-550, Brazil
Anderson Oliveira Lobo*
Affiliation:
LIMAV—Interdisciplinary Laboratory for Advanced Materials, UFPI—Federal University of Piaui, Teresina, Piauí 64049-550, Brazil
*
a)Address all correspondence to these authors. e-mail: josyosajima@ufpi.edu.br
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Abstract

In this work, filament based on ɛ-polycaprolactone (PCL) and containing the bioactive ceramics nanohydroxyapatite (nHap) and Laponite® (Lap) was prepared by the extrusion process. To obtain the material, a mass ratio of 89:10:1 (PCL:nHap:Lap) was used, and structural and morphological characterization was realized. In addition, cytotoxicity (using Allium cepa bulbs) and viability tests on L929 cells also were performed. The results showed that filament (diameter of 1.79 ± 0.17 mm) presented a good dispersion of nHap and Lap into polymeric matrices. Fourier transform infrared spectroscopy identified typical bands at 1720, 1091, and 1045 cm−1 addressed to PCL and nHAp, In addition, Lap was identified through dispersive energy system and X-ray diffraction analyses. All filaments did not exhibit cytotoxic effects.

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Article
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Copyright © Materials Research Society 2020

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Footnotes

c)

These authors contributed equally to this work.

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