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X-ray diffraction and high-resolution transmission electron microscopy study on A-site ordering of lanthanum-modified lead zirconate titanate relaxor

Published online by Cambridge University Press:  03 March 2011

Fei Fang  and
Xiaowen Zhang
Fei Fang
Affiliation:
Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, People's Republic of China
Xiaowen Zhang
Affiliation:
Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, People's Republic of China
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Abstract

The ordering behavior of La-modified lead zirconate titanate relaxor (PLZT 9/65/35) was investigated by use of an x-ray diffractometer (XRD) and high-resolution transmission electron microscopy (HRTEM). It was shown that a {h + 1/2, k + 1/2, 0}-type superlattice exists both in the x-ray diffraction pattern and selected area electron diffraction (SAED) image. High-resolution electron micrographs further demonstrated the existence of the superlattice and exposed the ordered and disordered regions in the lattice level. A model referring to an A-site body-centered pseudo-cubic superstructure was proposed.

Type
Rapid Communication
Information
Journal of Materials Research , Volume 10 , Issue 7 , July 1995 , pp. 1582 - 1584
Copyright
Copyright © Materials Research Society 1995

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References

REFERENCES

1Smolenskii, G. A., J. Phys. Soc. Jpn. 28 (Suppl.), 26–36 (1970).Google Scholar
2Setter, N. and Cross, L. E., J. Mater. Sci. 15, 2478–2482 (1980).CrossRefGoogle Scholar
3Setter, N. and Cross, L. E., J. Appl. Phys. 51(8), 4356–4360 (1980).CrossRefGoogle Scholar
4Krause, H. B., Cowley, J. M., and Whatley, J., Acta Crystallogr. A 35, 1015–1017 (1979).CrossRefGoogle Scholar
5Randall, C. A., Bhalla, A. S., Shrout, T. R., and Cross, L. E., J. Mater. Res. 5, 829–834 (1990).CrossRefGoogle Scholar
6Randall, C., Barber, D., Whatmore, R., and Croves, P., Ferroelectrics 76, 277–282 (1987).CrossRefGoogle Scholar
7Burns, G. and Dacol, F. H., Phys. Rev. B 28, 2527–2530 (1983).CrossRefGoogle Scholar
8Burns, G. and Dacol, F. H., Ferroelectrics 104, 25–35 (1990).CrossRefGoogle Scholar
9Darlington, C. N. W., J. Phys. C: Solid State Phys. 21, 3851–3861 (1988).CrossRefGoogle Scholar
10Gu, B. L., Zhang, X. W., Wang, Q., and Zhu, J. L., Jialim, Science in China (Series A) 34(7), 815–824 (1991).Google Scholar