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In Situ X-Ray Diffraction Studies of Crystallization Growth Behavior in ZnO-Bi2O3-B2O3 Glass as a Route to Functional Optical Devices

Published online by Cambridge University Press:  02 January 2018

Quentin Altemose ,
Katrina Raichle ,
Brittani Schnable ,
Casey Schwarz ,
Myungkoo Kang ,
Carlo Pantano ,
Kathleen Richardson  and
Clara Rivero-Baleine
Quentin Altemose
Affiliation:
Physics & Astronomy Department, Ursinus College, Collegeville, PA19426, U.S.A.
Katrina Raichle
Affiliation:
Physics & Astronomy Department, Ursinus College, Collegeville, PA19426, U.S.A.
Brittani Schnable
Affiliation:
Physics & Astronomy Department, Ursinus College, Collegeville, PA19426, U.S.A.
Casey Schwarz*
Affiliation:
Physics & Astronomy Department, Ursinus College, Collegeville, PA19426, U.S.A.
Myungkoo Kang
Affiliation:
CREOL, The College of Optics and Photonics, University of Central Florida, Orlando, FL32816, U.S.A.
Carlo Pantano
Affiliation:
Department of Materials Science and Engineering, Pennsylvania State University, University Park, PA16802, U.S.A.
Kathleen Richardson
Affiliation:
CREOL, The College of Optics and Photonics, University of Central Florida, Orlando, FL32816, U.S.A.
Clara Rivero-Baleine
Affiliation:
Lockheed Martin, Orlando, FL32819, U.S.A.
*
*(Email: cschwarz@ursinus.edu)
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Abstract

Transparent optical ZnO–Bi2O3–B2O3 (ZBB) glass-ceramics were created by the melt quenching technique. In this work, a melt of the glass containing stoichiometric ratios of Zn/Bi/B and As was studied. Differential scanning calorimeter (DSC) measurements was used to measure the thermal behavior. VIS/NIR transmission measurements were used to determine the transmission window. X-ray diffraction (XRD) was used to determine crystal phase. In this study, we explore new techniques and report a detailed study of in-situ XRD of the ZBB composition in order to correlate nucleation temperature, heat treatment temperature, and heat treatment duration with induced crystal phase.

Keywords

crystal growthnucleation & growthx-ray diffraction (XRD)
Type
Articles
Information
MRS Advances , Volume 3 , Issue 11: Theory, Characterization and Modeling , 2018 , pp. 563 - 567
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Copyright
Copyright © Materials Research Society 2017 

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References

Raichle, K., Schnable, B., Altemose, Q., Schwarz, C., Kang, M., Pantano, C., Richardson, K. and Rivero-Baleine, C., presented at the APS Conferences for Undergraduate Women in Physics Princeton, New Jersey, 2017 (unpublished).Google Scholar
Shanmugalevu, B. and Kumar, V.V., J. Am. Ceram. Soc., 85, 9, 2891–2898, (2012).Google Scholar
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