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Fabrication and testing of high-performance all-metal neutron guides and axisymmetric mirrors by electrochemical replication

Published online by Cambridge University Press:  27 February 2020

B. Khaykovich*
Affiliation:
Nuclear Reactor Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, U.S.A.
S. Romaine
Affiliation:
Center for Astrophysics | Harvard & Smithsonian, Cambridge, MA 02138, U.S.A.
A. Ames
Affiliation:
Center for Astrophysics | Harvard & Smithsonian, Cambridge, MA 02138, U.S.A.
R. Bruni
Affiliation:
Center for Astrophysics | Harvard & Smithsonian, Cambridge, MA 02138, U.S.A.
H. A. Ambaye
Affiliation:
Neutron Scattering Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN, U.S.A.
A. Glavic
Affiliation:
Neutron Scattering Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN, U.S.A.
V. Lauter
Affiliation:
Neutron Scattering Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN, U.S.A.
D. Engelhaupt
Affiliation:
Dawn Research, Huntsville, AL 35824, U.S.A.
*
(Email: bkh@mit.edu)
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Abstract

Neutron scattering is one of the most useful methods of studying the structure of matter, with applications to biomedical, structural, magnetic and energy-related materials. Neutron-scattering instruments are installed around research reactors or accelerator-based neutron sources, and neutron guides are critical components of these facilities. They are neutron-transport optical devices consisting of state-of-the-art mirrors often tens of meters long. Here we demonstrate a novel fabrication method of all-metallic neutron guides and axisymmetric mirrors by electroplating from precision mandrels. The process allows for the fabrication of single-piece all-metal guides of prismatic and axisymmetric shapes. We also demonstrate supermirror guides and axisymmetric focusing supermirrors produced with the same technology. We present the fabrication and tests of the multilayer-coated replicated guides and optic and show that the mandrel is reproduced with high fidelity and reliability. Such supermirror optics will provide game-changing improvements in neutron techniques.

Type
Articles
Copyright
Copyright © Materials Research Society 2020

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Footnotes

*

Currently at Stanford University, Stanford, CA, U.S.A.

Currently at The Paul Scherrer Institute, Villigen, Switzerland

References

REFERENCES

Maier-Leibnitz, H. and Springer, T., “The use of neutron optical devices on beam-hole experiments on beam-hole experiments,” J. Nucl. Energy Parts AB React. Sci. Technol., vol. 17, no. 4, pp. 217225, Jul. 1963, doi: 10.1016/0368-3230(63)90022-3.CrossRefGoogle Scholar
Mezei, F. and Dagleish, P., “Corrigendum and first experimental evidence on neutron supermirrors,” Commun. Phys. Lond., vol. 2, no. 2, pp. 4143, 1977.Google Scholar
Böni, P., “New concepts for neutron instrumentation,” Nucl. Instrum. Methods Phys. Res. Sect. Accel. Spectrometers Detect. Assoc. Equip., vol. 586, no. 1, pp. 18, Feb. 2008, doi: 10.1016/j.nima.2007.11.059.CrossRefGoogle Scholar
Pullen, S., Davidson, G., Pangalis, S., Klose, F., and Kennedy, S., “Report on the repair of the opal neutron beam transport system,” in Joint IGORR 2013 and IAEA Technology Meeting, 2013.Google Scholar
Schanzer, C., Böni, P., and Schneider, M., “High Performance Supermirrors on Metallic Substrates,” J. Phys. Conf. Ser., vol. 251, p. 012082, Nov. 2010, doi: 10.1088/1742-6596/251/1/012082.CrossRefGoogle Scholar
Fawcett, S. C. and Engelhaupt, D., “Development of Wolter I x-ray optics by diamond turning and electrochemical replication,” Precis. Eng., vol. 17, no. 4, pp. 290297, Oct. 1995, doi: 10.1016/0141-6359(95)00018-9.CrossRefGoogle Scholar
Ramsey, B. D., “Replicated Nickel Optics for the Hard-X-Ray Region,” Exp. Astron., vol. 20, no. 1, pp. 8592, 2005.CrossRefGoogle Scholar
Khaykovich, B., Gubarev, M. V., Bagdasarova, Y., Ramsey, B. D., and Moncton, D. E., “From X-ray telescopes to neutron scattering: Using axisymmetric mirrors to focus a neutron beam,” Nucl. Instrum. Methods Phys. Res. Sect. Accel. Spectrometers Detect. Assoc. Equip., vol. 631, no. 1, p. 98, 2011.CrossRefGoogle Scholar
Mezei, F., “Novel polarized neutron devices: supermirror and spin component amplifier,” Commun. Phys. Lond., vol. 1, no. 3, pp. 8185, 1976.Google Scholar
Liu, D. et al., “Demonstration of Achromatic Cold-Neutron Microscope Utilizing Axisymmetric Focusing Mirrors,” App Phys Lett, vol. 102, p. 183508, 2013.CrossRefGoogle Scholar
Liu, D. et al., “Response to ‘Comment on “Demonstration of achromatic cold-neutron microscope utilizing axisymmetric focusing mirrors”’ [Appl. Phys. Lett. 103, 236101 (2013)],” Appl. Phys. Lett., vol. 103, no. 23, p. 236102, 2013, doi: 10.1063/1.4835175.CrossRefGoogle Scholar
Jorba, P. et al., “High-resolution neutron depolarization microscopy of the ferromagnetic transitions in Ni3Al and HgCr2Se4 under pressure,” J. Magn. Magn. Mater., vol. 475, pp. 176183, Apr. 2019, doi: 10.1016/j.jmmm.2018.11.086.CrossRefGoogle Scholar
Hussey, D. et al., “Demonstration of Focusing Wolter Mirrors for Neutron Phase and Magnetic Imaging,” J. Imaging, vol. 4, no. 3, p. 50, Mar. 2018, doi: 10.3390/jimaging4030050.CrossRefGoogle Scholar
Wu, H., Khaykovich, B., Wang, X., and Hussey, D. S., “Wolter Mirrors for Neutron Imaging,” Phys. Procedia, vol. 88, pp. 184189, 2017, doi: 10.1016/j.phpro.2017.06.025.CrossRefGoogle Scholar
Liu, D., Gubarev, M. V., Resta, G., Ramsey, B. D., Moncton, D. E., and Khaykovich, B., “Axisymmetric Grazing-Incidence Focusing Optics for Small-Angle Neutron Scattering,” Nucl Instrum Methods Phys Res A, vol. 686, pp. 145150, 2012.CrossRefGoogle Scholar
Liu, D. et al., “Demonstration of a novel focusing small-angle neutron scattering instrument equipped with axisymmetric mirrors,” Nat. Commun., vol. 4, p. 2556, 2013.CrossRefGoogle ScholarPubMed
Romaine, S. et al., “Mandrel replication for hard x-ray optics using titanium nitride,” Proc. SPIE, vol. 7437, p. 74370Y, 2009.CrossRefGoogle Scholar
Romaine, S., Boike, J., Bruni, R., Engelhaupt, D., Gorenstein, P., and Ramsey, B., “Improved release coatings for electroformed x-ray optics,” 2011, vol. 8147, pp. 81470W-81470W–6, doi: 10.1117/12.896000.CrossRefGoogle Scholar
Citterio, O., Conconi, P., Ghigo, M., Mazzoleni, F., Pareschi, G., and Peverini, L., “Development of soft and hard x-ray optics for astronomy,” presented at the International Symposium on Optical Science and Technology, San Diego, CA, USA, 2000, p. 43, doi: 10.1117/12.407566.CrossRefGoogle Scholar
Engelhaupt, D. E., Ramsey, B. D., O’Dell, S. L., Jones, W. D., and Russell, J. K., “New alloys for electroformed replicated x-ray optics,” presented at the International Symposium on Optical Science and Technology, San Diego, CA, USA, 2000, p. 154, doi: 10.1117/12.407555.CrossRefGoogle Scholar
Ramsey, B. D. et al., “The development of hard X-ray optics at MSFC,” Proc. SPIE, vol. 4851, pp. 631638, 2003.CrossRefGoogle Scholar
Hayter, J. B. and Mook, H. A., “Discrete thin-film multilayer design for X-ray and neutron supermirrors,” J. Appl. Crystallogr., vol. 22, no. 1, pp. 3541, Feb. 1989, doi: 10.1107/S0021889888010003.CrossRefGoogle Scholar
Lauter, V., Ambaye, H., Goyette, R., Hal Lee, W.-T., and Parizzi, A., “Highlights from the magnetism reflectometer at the SNS,” Phys. B Condens. Matter, vol. 404, no. 17, pp. 25432546, Sep. 2009, doi: 10.1016/j.physb.2009.06.021.CrossRefGoogle Scholar
Windt, D. L., “IMD—Software for modeling the optical properties of multilayer films,” Comput. Phys., vol. 12, no. 4, p. 360, 1998, doi: 10.1063/1.168689.CrossRefGoogle Scholar
Lauter, V., Lauter, H., Glavic, A., and Toperverg, B., Reference module in materials science and materials engineering. Elsevier, 2016.Google Scholar
Lauter-Pasyuk, V., “Neutron grazing incidence techniques for nano-science,” Collect. SFN, vol. 7, pp. s221s240, 2007.CrossRefGoogle Scholar
Yoneda, Y., “Anomalous surface reflection of X rays,” Phys. Rev., vol. 131, no. 5, p. 2010, 1963.Google Scholar
Khaykovich, B., Liu, D., Moncton, D. E., Gubarev, M. V., and Ramsey, B. D., “A new generation of neutron-focusing optics,” SPIE Newsroom, Feb. 2014, doi: 10.1117/2.1201401.005243.CrossRefGoogle Scholar
Khaykovich, B., Liu, D., Resta, G., Moncton, D. E., and Gubarev, M. V., “On the challenge of flux concentration at grazing incidence for neutrons and x-rays,” in SPIE Optical Engineering Applications, 2012, vol. 8485, pp. 848509-848509–6.Google Scholar