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The Application of Atomic Force Microscopy to the Characterization of Industrial Polymer Materials

Published online by Cambridge University Press:  31 January 2011

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Abstract

Atomic force microscopy (AFM) is now well established among the tools of choice for the analysis and characterization of materials.Applications of AFM span many industries including chemicals, plastics, pharmaceuticals, and semiconductors.Advancements in AFM instrumentation over the last five years have expanded the range of application of this technology to investigate thermal and mechanical properties of complex materials at high spatial resolution as well as structural and morphological characterization of materials subjected to thermal and mechanical stresses.In particular, this has been an enabling technology for an improved understanding of structure–property relationships in polymeric materials including homopolymers, blends, impact-modified polymer systems, porous polymer systems, and semicrystalline polymers.Practical examples illustrate applications of contact, tapping-mode, phase-imaging, hot-stage, and scanning thermal methods for the characterization of modern industrial polymer materials.

Type
Research Article
Copyright
Copyright © Materials Research Society 2004

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References

1Binnig, G., Quate, C., and Gerber, Ch., Phys. Rev. Lett. 56 (1986) p.930.CrossRefGoogle Scholar
2Zhong, Q., Innis, D., Kjoller, K., and Elings, V., Surf. Sci. Lett. 290 (1993) p.L688.Google Scholar
3Chernoff, D.A., in Proc. Microscopy and Microanalysis (Jones and Bagell, New York, 1995) p.888.Google Scholar
4Ivanov, D., Daniels, R., and Magonov, S., “Exploring the High-Temperature AFM and Its Use for Studies of Polymers,” Application Note, Digital Instruments/Veeco Metrology Group, http://www.veeco.com/appnotes/AN45_ HeatingStage.pdf (accessed April 2004).Google Scholar
5D'Orazio, L., Mancarella, C., Martuscelli, E., and Polato, F., Polymer 32 (1991) p.1186.CrossRefGoogle Scholar
6Wal, A. Van der, Nijhof, R., and Gaymans, R.J., Polymer 40 (1999) p.6031.Google Scholar
7Carriere, C.J. and Silvis, H.C., J. Appl. Polym. Sci. 66 (1997) p.1175.3.0.CO;2-0>CrossRefGoogle Scholar
8Bucknall, C.B., Toughened Plastics (Applied Science, London, 1977).CrossRefGoogle Scholar
9Premphet, K. and Paecharoenchai, W., J.Appl. Polym. Sci. 82 (2001) p.2140.CrossRefGoogle Scholar
10Thomann, Y., Thomann, R., Bar, G., Ganter, M., Machutta, B., and Mülhaupt, R., J. Microsc. 195 (1999) p.161.CrossRefGoogle Scholar
11Russ, J.C.B., Computer-Assisted Microscopy: The Measurement and Analysis of Images (Plenum Press, New York, 1990).CrossRefGoogle Scholar
12Padden, F.J. and Keith, H.D., J.Appl. Phys. 44 (1973) p.1217.CrossRefGoogle Scholar
13Meile, S.V., Ferro, D.R., Brückner, S., Lovinger, A.J., and Padden, F. J., Macromolecules 319 (1994) p.187.Google Scholar
14Brückner, S. and Meile, S.V., Nature 340 (1989) p.455.Google Scholar
15Brückner, S., Meile, S.V., Petraccone, V., and Pirozzi, B., Prog. Polym. Sci. 16 (1991) p.361.CrossRefGoogle Scholar
16Lotz, B. and Wittmann, J.C., Prog. Colloid Polym. Sci. 87 (1992) p.3.Google Scholar
17Hamley, I., The Physics of Block Copolymers (Oxford University Press, Oxford, 1998).CrossRefGoogle Scholar
18Cieslinski, R., Hahn, S., Hahnfeld, J., Jones, M.A., Leibig, C., Milhaupt, J., Meyers, G., Landes, B., Langhoff, C., Parsons, G., Reinhardt, M., and Yontz, D., Polymer Preprints, Vol. 43, No. 1 (American Chemical Society, Washington, DC, 2002) p.289.Google Scholar
19Ruokolainen, J., Fredrickson, G., Kramer, E., Ryu, C., Hahn, S., Magonov, S., Macromolecules 35 (2002) p.9391.CrossRefGoogle Scholar
20Hammond, M., Sides, S., Frederickson, G., Kramer, E., Macromolecules 36 (2003) p.8712.CrossRefGoogle Scholar
21Magonov, S., Cleveland, J., Elings, V., Denley, D., Whangbo, M.-H., Surface Science 389 (1997) p.201.CrossRefGoogle Scholar
22Pollock, H.M. and Hammiche, A., J.Phys. D: Appl. Phys. 34 (1) (2001) p.R23.CrossRefGoogle Scholar
23Lever, T. and Price, D., American Laboratory 30 (16) (1998) p.15.Google Scholar
24Product Focus: LDPE,” Chemical Week 165 (19) (2003) p.36.Google Scholar