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Three-dimensional analysis of dendrites via automated serial sectioning using a Robo-Met.3D

Published online by Cambridge University Press:  18 June 2020

Y. Lu ,
M. Wang ,
Z. Wu ,
I. P. Jones ,
M. Wickins ,
N. R. Green  and
H. C. Basoalto
Y. Lu*
Affiliation:
School of Metallurgy and Materials, University of Birmingham, Edgbaston, BirminghamB15 2TT, UK
M. Wang
Affiliation:
School of Metallurgy and Materials, University of Birmingham, Edgbaston, BirminghamB15 2TT, UK
Z. Wu
Affiliation:
School of Metallurgy and Materials, University of Birmingham, Edgbaston, BirminghamB15 2TT, UK
I. P. Jones
Affiliation:
School of Metallurgy and Materials, University of Birmingham, Edgbaston, BirminghamB15 2TT, UK
M. Wickins
Affiliation:
School of Metallurgy and Materials, University of Birmingham, Edgbaston, BirminghamB15 2TT, UK High Temperature Research Centre (HTRC), University of Birmingham, Unit 2 Airfield Drive, Ansty Business Park, CoventryCV7 9BF, UK
N. R. Green
Affiliation:
School of Metallurgy and Materials, University of Birmingham, Edgbaston, BirminghamB15 2TT, UK High Temperature Research Centre (HTRC), University of Birmingham, Unit 2 Airfield Drive, Ansty Business Park, CoventryCV7 9BF, UK
H. C. Basoalto
Affiliation:
Department of Materials Science and Engineering, The University of Sheffield, Mappin Street, SheffieldS1 3JD, UK
*
Address all correspondence to Y. Lu at y.lu.2@bham.ac.uk
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Abstract

The dendrite morphologies of the cast nickel-based superalloy CMSX-4® (CMSX-4® is registered trademarks of the Cannon-Muskegon Corporation) and the austenitic stainless steel HP microalloy have been obtained via an automated serial-sectioning process which allows three-dimensional (3D) microstructural characterization. The dendrite arm spacing, volume fraction of segregation, and fraction of porosity have been determined. This technique not only increases the depth, scope, and level of detailed microstructural characterization but also delivers microstructural data for modeling and simulation.

Type
Research Letters
Information
MRS Communications , Volume 10 , Issue 3 , September 2020 , pp. 461 - 466
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Copyright
Copyright © Materials Research Society, 2020

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References

Ardakani, M.G., D'Souza, N., Wagner, A., Shollock, B.A., and McLean, M.: Competitive grain growth and texture evolution during directional solidification of superalloys. In Superalloys 2000. TMS (The Minerals, Metals & Materials society), 219–228 (2000).Google Scholar
Huang, S.C. and Glicksman, M.E.: Overview 12: Fundamentals of dendritic solidification-II development of sidebranch structure. Acta Metall. 29, 717–734 (1981).CrossRefGoogle Scholar
Osório, W.R., Goulart, P.R., Santos, G.A., Neto, C.M., and Garcia, A.: Effect of dendritic arm spacing on mechanical properties and corrosion resistance of Al 9 wt pct Si and Zn 27 wt pct Al alloys. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 37, 2525–2538 (2006).CrossRefGoogle Scholar
Goulart, P.R., Osório, W.R., Spinelli, J.E., and Garcia, A.: Dendritic microstructure affecting mechanical properties and corrosion resistance of an Al-9 wt% Si alloy. Mater. Manuf. Process. 22, 328–332 (2007).CrossRefGoogle Scholar
Quested, P.N. and McLean, M.: Solidification morphologies in directionally solidified superalloys. Mater. Sci. Eng. 65, 171–180 (1984).CrossRefGoogle Scholar
Wu, X.Q., Jing, H.M., Zheng, Y.G., Yao, Z.M., Ke, W., and Hu, Z.Q.: The eutectic carbides and creep rupture strength of 25Cr20Ni heat-resistant steel tubes centrifugally cast with different solidification conditions. Mater. Sci. Eng. A 293, 252–260 (2000).CrossRefGoogle Scholar
Voicu, R., Lacaze, J., Andrieu, E., Poquillon, D., and Furtado, J.: Creep and tensile behaviour of austenitic Fe-Cr-Ni stainless steels. Mater. Sci. Eng. A 510–511, 185–189 (2009).CrossRefGoogle Scholar
Bruckner, U., Epishin, A., and Link, T.: Local X-ray diffraction analysis of the structure of dendrites in single-crystal nickel-base superalloys. Acta Mater. 45, 5223–5231 (1997).CrossRefGoogle Scholar
Guo, E., Phillion, A.B., Cai, B., Shuai, S., Kazantsev, D., Jing, T., and Lee, P.D.: Dendritic evolution during coarsening of Mg-Zn alloys via 4D synchrotron tomography. Acta Mater. 123, 373–382 (2017).CrossRefGoogle Scholar
Lamm, M. and Singer, R.F.: The effect of casting conditions on the high-cycle fatigue properties of the single-crystal nickel-base superalloy PWA 1483. Metall. Mater. Trans. A 38, 1117–1183 (2007).CrossRefGoogle Scholar
Wang, M.Y., Williams, J.J., Jiang, L., Carlo, F.D., Jing, T., and Chawla, N.: Dendritic morphology of α-Mg during the solidification of Mg-based alloys: 3D experimental characterization by X-ray synchrotron tomography and phase-field simulations. Scr. Mater. 65, 855–858 (2011).CrossRefGoogle Scholar
Alkemper, J. and Voorhees, P.W.: Quantitative serial sectioning analysis. J. Microsc. 201, 388–394 (2001).CrossRefGoogle ScholarPubMed
Maruyama, B., Spowart, J.E., Hooper, D.J., Mullens, H.M., Druma, A.M., Druma, C., and Alam, M.K.: A new technique for obtaining three-dimensional structures in pitch-based carbon foams. Scr. Mater. 54, 1709–1713 (2006).CrossRefGoogle Scholar
Zhou, X., Luo, C., Hashimoto, T., Hughes, A.E., and Thompson, G.E.: Study of localized corrosion in AA2024 aluminium alloy using electron tomography. Corros. Sci. 58, 299–306 (2012).CrossRefGoogle Scholar
Uchic, M.D., Groeber, M.A., Dimiduk, D.M., and Simmons, J.P.: 3D microstructural characterization of nickel superalloys via serial-sectioning using a dual beam FIB-SEM. Scr. Mater. 55, 23–28 (2006).CrossRefGoogle Scholar
Lu, Y., Chiu, Y.L. and Jones, I.P.: Three-dimensional analysis of the microstructure and bio-corrosion of Mg-Zn and Mg-Zn-Ca alloys. Mater. Charact. 112, 113–121 (2016).CrossRefGoogle Scholar
Witte, F., Fischer, J., Beckmann, F., Störmer, M., and Hort, N.: Three-dimensional microstructural analysis of Mg-Al-Zn alloys by synchrotron-radiation-based microtomography. Scr. Mater. 58, 453–456 (2008).CrossRefGoogle Scholar
Kübel, C., Voigt, A., Schoenmakers, R., Otten, M., Su, D., Lee, T.C., Carlsson, A., and Bradley, J.: Recent advances in electron tomography: TEM and HAADF-STEM tomography for materials science and semiconductor applications. Microsc. Microanal. 11, 378–400 (2005).CrossRefGoogle ScholarPubMed
Spowart, J.E., Mullens, H.E., and Puchala, B.T.: Collecting and analyzing microstructures in three dimensions: a fully automated approach. J. Miner. 55, 35–37 (2003).Google Scholar
Brener, E.: Needle-crystal solution in three-dimensional dendritic growth. Phys. Rev. Lett. 71, 3653–3656 (1993).CrossRefGoogle ScholarPubMed
Martin, O. and Goldenfeld, N.: Origin of sidebranching in dendritic growth. Phys. Rev. A 35, 1382–1390 (1987).CrossRefGoogle ScholarPubMed
Brener, E. and Temkin, D.: Noise-induced sidebranching in the three-dimensional nonaxisymmetric dendritic growth. Phys. Rev. E 51, 351–359 (1995).CrossRefGoogle ScholarPubMed
Jeong, J.H., Goldenfeld, N., and Dantzig, J.A.: Phase field model for three-dimensional dendritic growth with fluid flow. Phys. Rev. E 64, 041602 (2001).CrossRefGoogle ScholarPubMed
Madison, J., Spowart, J.E., Rowenhorst, D.J., and Pollock, T.M.: The three-dimensional reconstruction of the dendritic structure at the solid-liquid interface of a Ni-based single crystal. JOM 60, 26–30 (2008).CrossRefGoogle Scholar
Madison, J., Spowart, J.E., Rowenhorst, D.J., Fiedler, J., and Pollock, T.M.: Characterization of three-dimensional dendritic structures in nickel-base single crystals for investigation of defect formation. Superalloys 881–888 (2008).Google Scholar
Madison, J., Spowart, J.E., Rowenhorst, D.J., Aagesen, L.K., Thornton, K., and Pollock, T.M.: Fluid flow and defect formation in the three-dimensional dendritic structure of nickel-based single crystals. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 43, 369–380 (2012).CrossRefGoogle Scholar
Lorensen, W.E. and Cline, H.E.: Marching cubes: A high resolution 3D surface construction algorithm. Comput. Graph. 21, 163–169 (1987).CrossRefGoogle Scholar
Velichko, A., Holzapfel, C., and Mücklich, F.: 3D characterization of graphite morphologies in cast iron. Adv. Eng. Mater. 9, 39–45 (2007).CrossRefGoogle Scholar