Hostname: page-component-78c5997874-v9fdk Total loading time: 0 Render date: 2024-11-10T10:30:03.538Z Has data issue: false hasContentIssue false

Bright plasma nitriding of ferritic steel with several alloying elements

Published online by Cambridge University Press:  11 February 2011

J.-D. Kamminga
Affiliation:
Netherlands Institute for Metals Research, Delft, Netherlands, e-mail: J.D.Kamminga@tnw.tudelft.nl
C. Kwakernaak
Affiliation:
Department of Materials Science and Technology, Delft University of Technology, Netherlands
G. C. A. M. Janssen
Affiliation:
Department of Materials Science and Technology, Delft University of Technology, Netherlands
Get access

Abstract

Hot work tool steel was plasma nitrided in a PVD apparatus. Phases occurring and nitrogen depth profiles were assessed for the nitrided specimens. In all cases bright nitriding was achieved. Increasing the nitriding time from 15 to 120 min yielded a nitriding depth increasing from about 15 to 35 μm, whereas the nitrogen flux decreased from 8.0 to 5.5 × 10-7 kg s-1m-2. Results from an existing model, predicting nitrogen depth profiles due to plasma nitriding, did not accurately describe the experimental data. Therefore the existing model cannot be used straightforwardly to predict the formation of iron nitrides. The discrepancies of model results and experimental results are discussed in view of the assumptions underlying the model for plasma nitriding.

Type
Research Article
Copyright
Copyright © Materials Research Society 2003

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Sun, Y., Bell, T., Trans. Inst. Metal Finish. 70, 38 (1992).Google Scholar
2. Sun, Y., Bell, T., Mater. Sci. Eng. A140, 419 (1991).Google Scholar
3. Dingremont, N., Pianelli, A., Bergmann, E., Michel, H., Surf. Coat. Technol. 61, 187 (1993).Google Scholar
4. Somers, M.A.J., Lankreijer, R.M., Mittemeijer, E.J., Phil. Mag. A59, 353 (1989).Google Scholar
5. Lankreijer, R.M., Somers, M.A.J., and Mittemeijer, E.J. in Proc. Int. Conf. on High Nitrogen Steels, Lille, France, May 18–20 1988, edited by Foct, J. and Hendry, A. (The Institute of Metals, London, 1989), pp. 108111.Google Scholar
6. Sun, Y., Bell, T., Mater. Sci. Eng. A224, 33 (1997).Google Scholar
7. Sun, Y., Bell, T., Heat Treatment of Metals Vol. 24 No. 2, 43 (1997).Google Scholar
8. Gouné, M., Belmonte, T., Chomer, S., Michel, H., Thin Solid Films 377–378, 543 (2000).Google Scholar
9. Kamminga, J.-D., Hoy, R., Janssen, G.C.A.M., submitted to Surf. Coat. Technol. (2002).Google Scholar
10. Janssen, G.C.A.M., Kamminga, J.-D., and Sloof, W.G. in Nanophase and Nanocomposite Materials IV, edited by Komarneni, S., Vaia, R.A., Lu, G.Q., Matsushita, J-I., and Parker, J.C., (Mater. Res. Soc. Proc. 703, Warrendale PA, 2001) pp. 153158.Google Scholar
11. Mortimer, B., Grieveson, P., Jack, K.H., Scand. J. Metallurgy 1, 203 (1972).Google Scholar
12. Oriani, R.A., Acta Metall. 18, 147 (1970).Google Scholar