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Advanced TEM Investigations on Ni-Ti Shape Memory Material: Strain and Concentration Gradients Surrounding Ni4Ti3 Precipitates

Published online by Cambridge University Press:  26 February 2011

Dominique Schryvers
Affiliation:
Electron Microscopy for Materials Science (EMAT), University of Antwerp, Groenenborgerlaan 171, B-2020 Antwerpen, Belgium
Wim Tirry
Affiliation:
Electron Microscopy for Materials Science (EMAT), University of Antwerp, Groenenborgerlaan 171, B-2020 Antwerpen, Belgium
Zhiqing Yang
Affiliation:
Electron Microscopy for Materials Science (EMAT), University of Antwerp, Groenenborgerlaan 171, B-2020 Antwerpen, Belgium
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Abstract

Lattice deformations and concentration gradients surrounding Ni4Ti3 precipitates grown by appropriate annealing in a Ni51Ti49 B2 austenite matrix are determined by a combination of TEM techniques. Quantitative Fourier analysis of HRTEM images reveals a deformed nanoscale region with lattice deformations up to 2% while EELS and EDX indicate a Ni depleted zone up to 150 nm away from the matrix-precipitate interface.

Type
Research Article
Copyright
Copyright © Materials Research Society 2005

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References

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