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Published online by Cambridge University Press: 26 February 2011
In this study, we are demonstrating localized nano-scale analysis of sensor materials which are developed using combinatorial gradient approach. Our technique based on Focused Ion Beam cross-sectioning at specific locations affords establishing metal nano-particles concentrations at best-performing area(s) of gradient-formulated polymer samples. We have achieved three-dimensional characterization/mapping of nano-fillers (30-100 nm metal particles) in composite thin films on variety of substrates.