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Interface Characterisation Using an SEM-Based Micro-Indentor

Published online by Cambridge University Press:  15 February 2011

M.H. Lewis
Affiliation:
Centre for Advanced Materials, University of Warwick, Coventry, CV4 7AL, UK
A.M. Daniel
Affiliation:
C.E.I.T., 20080, San-Sebastian, Spain
M.G. Cain
Affiliation:
Centre for Advanced Materials, University of Warwick, Coventry, CV4 7AL, UK
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Abstract

The design and performance of an SEM-based microindentor, for interfacial property measurements in CMCs, is described. It enables high resolution imaging and simultaneous load/displacement monitoring with capacity and resolution of 20N ± lmN (load) and 100μm ± 10nm (displacement). Its application to measurement of interface debond and shear stresses for a wide range of fibres and monofilaments is described.

Type
Research Article
Copyright
Copyright © Materials Research Society 1995

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References

1. Shafry, N., Brandon, D.G., Proc. 7th CIMTEC, Terme, Italy. June 27-30, (1990).Google Scholar
2. Marshall, D.B., Oliver, W.C., J. Am. Ceram. Soc., 70, 542, (1987).Google Scholar
3. Weihs, T.P., Nix, W.D., Scripta. Metall. et Mat., 22, 271, (1988).Google Scholar
4. Evans, A.G., AGARD-R-795, paper 2, (1993).Google Scholar
5. Daniel, A.M., Smith, S.T., Lewis, M.H., Rev. Sci. Instr, 65, 632 (1994).Google Scholar
6. Razzell, A.G., Lewis, M.H., J. Microscopy, 169, 215, (1993).Google Scholar
7. Lewis, M.H., Daniel, A.M., Chamberlain, A., Pharaoh, M.W., Cain, M.G., J. Microscopy, 169, 109, (1993).Google Scholar
8. Pharaoh, M.W., Daniel, A.M., Lewis, M.H., J. Mater. Lett. 12, 9981001, (1993).Google Scholar
9. Allen, R.F., Daniel, A.M., Lewis, M.H., Bowen, P., Scripta Metall. in press.Google Scholar