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Nanoscratch Deformation Response of Carbon Nitride Thin Films
Published online by Cambridge University Press: 17 March 2011
Abstract
The mechanical performance of thin carbon nitride (CNx) films deposited onto Si(100) substrate by sputtering, was investigated in the load range of 2-20 mN using nanoindentation and nanoscratch techniques. The microstructure of these films was characterized by the inhomogeneous embedding of crystalline grains into a N-poor amorphous matrix. A load dependent transition was found in both the scratch, as well as the friction responses. Below 5 mN, nanoscratching showed completely elastic behavior of the film, while above 10 mN a mixed elastic-plastic behavior was identified. Testing under a normal load of 20 mN resulted in local grooving at the film surface; however, in-situ profiling of the scratch trace showed no evidence of film failure. Both the coefficient of friction (μ), as well as the plastic deformation of the films were found increasing with the normal load applied following an exponential low.
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- Copyright © Materials Research Society 2001