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Polycrystalline Lead Iodide Films: Optical, Electrical and X-ray Counting Characterization

Published online by Cambridge University Press:  17 March 2011

L. Fornaro ,
E. Saucedo ,
L. Mussio ,
A. Gancharov ,
F. Guimaraes  and
A. Hernandes
L. Fornaro
Affiliation:
Radiochemistry Department, Faculty of Chemistry, Montevideo, URUGUAY
E. Saucedo
Affiliation:
Radiochemistry Department, Faculty of Chemistry, Montevideo, URUGUAY
L. Mussio
Affiliation:
Radiochemistry Department, Faculty of Chemistry, Montevideo, URUGUAY
A. Gancharov
Affiliation:
Radiochemistry Department, Faculty of Chemistry, Montevideo, URUGUAY
F. Guimaraes
Affiliation:
Instituto de Fisica de Sao Carlos, Universidade de Sao Paulo, SP, BRASIL
A. Hernandes
Affiliation:
Instituto de Fisica de Sao Carlos, Universidade de Sao Paulo, SP, BRASIL
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Abstract

Lead iodide purified by zone refining and repeated sublimation was used for growing Polycrystalline films by physical vapor deposition. Palladium film was deposited as rear contact onto glass and alumina substrates 2.5 × 2.5 cm2 in size. Onto it, lead iodide polycrystalline films were grown by sublimation at 390 °C and 5 × 10−5 mm Hg, substrate temperatures of about 200 °C and deposition times of about 10 days. Film thickness was measured by X-ray transmission at 59.5 keV giving values from 35 to 50 μm (5%). Optical and atomic force microscopy were performed to the films giving an average grain size of (80±20) μm. Low temperature photoluminescence was performed and peak position and broadness confirmed the high purity of starting materials. Films were characterized by X-ray diffraction, giving an [ΣI (0 0 l)] / [ΣI (h k l)] relation of 0.8 that indicates a strong growth preferred orientation along c axis. Front palladium thermal deposition contacts and acrylic encapsulation were done and apparent resistivity (2 × 1014 Ω. cm) and current density (7 pA/cm2 (30 V)) were obtained. X-ray film response was checked by irradiating with 241Am and an X-ray beam. Finally, film and detector characterizations were correlated with starting material, deposition parameters and previous results for the same and alternative materials like mercuric iodide.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 685: Symposium D – Advanced Materials and Devices for Large-Area Electronics , 2001 , D5.7.1
Copyright
Copyright © Materials Research Society 2001

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References

1. Wiestfield, R.L., Hartney, M.A., Street, R.A. and Apte, R.B., Proceedings of SPIE 3336, 444 (1998).Google Scholar
2. Rahn, T.J., Lemmi, F., Lu, J.P., Mei, P., Apte, R.B., Street, R.A., Lujan, R., Wiestfield, R.L. and Heanue, J.A., IEEE Transactions on Nucl. Sci. 46, 3, 457 (1999).Google Scholar
3. Antonuk, L.E., El-Mohri, Y., Hall, A., Jee, K.W., Maolinbay, M., Nassif, S.C., Rong, X., Siewerdsen, J.H., Zhao, Q. and Weisfield, R.L., Proceedings of SPIE 3336, 2 (1998).Google Scholar
4. Bennet, P.R., Shah, K.S., Cirignano, L.J., Klugerman, M.B., Moy, L.P. and Squillante, M.R., IEEE Transactions on Nucl. Sci. 46, 3, 266 (1999).Google Scholar
5. Pulichuk, P., Rougeot, H., Wong, K., Debrie, A., Poliquin, E., Hansroul, M., Martin, J.P., Troung, T.P., Choquette, M., Laperrere, L. and Shukri, Z., Proceedings of SPIE 3659, 417 (1999).Google Scholar
6. Shah, K.S., Bennet, P., Cirignano, L., Dmitriyev, Y., Klugerman, M., Mandal, K., Moy, L.P. and Street, R.A., Mat. Res. Soc. Symp. Proc. 487, 351 (1998).Google Scholar
7. Street, R.A., Rahn, J.T., Ready, S.E., Shah, K., Bennet, P.R., Dimitriyev, Y., Mei, P., Lu, J.P., Apte, R.B., Ho, J., Schylenbergh, K., Lemmi, F., Boyce, J.B. and Nylen, P., Proceedings of SPIE 3659, 36 (1999).Google Scholar
8. Shah, K.S., Bennet, P., Dmitriyev, Y., Cirignanno, L., Klugerman, M., Squillante, M.R., Street, R.A., Rahn, J.T. and Ready, S.E., Proceedings of SPIE 3770 (1999) 164.Google Scholar
9. Schieber, M., Zuck, A., Braiman, M., Melekhov, L., Nissenbaum, J., Turchetta, R., Dulinski, W., Husson, D., Riester, J.L., Schlesinger, T.E., Toney, J., Sanguinetti, S., Montalti, M. and Guzzi, M., Mat. Res. Soc. Symp, Proc. 487, 329 (1998).Google Scholar
10. Schieber, M., Zuck, A., Melenkhov, L., Shatunovsky, R., Hermon, H. and Turchetta, R., Proceedings of SPIE 3768, 296 (1999).Google Scholar
11. Schieber, M., Hermon, H., Zuck, A., Vilensky, A., Melekhov, L., Shatunovsky, R., Meerson, E. and Saado, H., Proceedings of SPIE 3770, 146 (1999).Google Scholar
12. Street, R. A., Mulato, M., Ready, S.E., Lau, R., Ho, J., VanSchuylenbergh, K., Schieber, M., Hermon, H., Zuck, A. and Vilensky, A., Proceedings of SPIE 4142,189 (2000).Google Scholar
13. Fornaro, L., Saucedo, E., Mussio, L., Yerman, L., Ma, X. and Burger, A., Nucl. Instrum. Meth. in Phys. Res. A 458/1–2, 406, (2001).Google Scholar
14. Iwanczyk, J.S., Patt, B.E., Tull, C.R., Donald, L.R. Mac, Skinner, N., Hoffman, E.J. and Fornaro, L., Presented at the 2000 IEEE NSS-MIC Conference, 2000, Lyon, France.Google Scholar
15. Hubbell, J. H., and Seltzer, S. M., Tables of X-Ray Mass Attenuation Coefficients and Mass Energy-Absorption Coefficients from 1 keV to 20 MeV for Elements Z = 1 to 92 and 48 Additional Substances of Dosimetric Interest, NISTIR 5632, National Institute of Standards and Technology, USA, 1996.Google Scholar
16. Lund, J.C., Olshner, F. and Burger, A. in Semiconductors for Room Temperature Nuclear Detector Applications, Semiconductors and Semimetals Vol. 43. Edited by Schlesinger, T.E. and James, R.B. (Academic Press, Inc., San Diego, CA, USA, 1995), pags. 445, 98.Google Scholar
17. Ferreira da Silva, A., Veissid, N. and Batista da Silva, A.V., Appl. Phys. Lett. 69 (13), 1930 (1996).Google Scholar
18. Deich, V. and Roth, M., Nucl. Instr. and Meth. in Phys. Res. A380,169 (1996).Google Scholar
19. Pfann, W.G. Zone melting. Robert E. Kreiger Publishing, Huntington, NY, 1978.Google Scholar
20. Eckstein, J., Erler, B. and Benz, K., Mat. Res. Bull., 27,537 (1992).Google Scholar
21. Schlesinger, T.E., James, R. B., Schieber, M., Toney, J., Scyoc, J.M. Van, Salary, L., Hermon, H., Lund, J., Buger, A., Chen, KT, Cross, E., Soria, E., Shah, K., Squillante, M., Yoon, H. and Goorsky, M., Nucl. Instr. and Meth. in Phys. Res. A380, 193 (1996).Google Scholar
22. , Hermon, James, R.B., Lund, J., Cross, E., Antolak, A., Morse, D.H., Medlin, D.L., Soria, E., Scyoc, J. Van, Brunett, B., Schieber, M., Schlesinger, T.E., Toney, J., Goorsky, M., Yoon, H., Burger, A., Salary, L., Chen, K-T., Y-C. Chang and Shah, K., Mat. Res. Soc. Symp. Proc. 487, 361 (1998).Google Scholar
23. Chen, K-T., Burger, A., Chen, H., Chen, Y-F., Hansen, K., Suber, L., Wilson, S., Henderson, J., Wright, G.W. and Cole, M.L., Mat. Res. Soc. Symp. Proc. 487, 369 (1998).Google Scholar
24. Lund, J., Shah, K., Squillante, M., Moy, L., Sinclair, F. and Entine, G., Nucl. Instr. and Meth. in Phys. Res. A283, 299 (1989).Google Scholar
25. “New ways for purifying lead iodide appropriate as spectrometric grade material”, Fornaro, L., Saucedo, E., Mussio, L., Gancharov, A., sent to J. of Mat. Sci., 2001.Google Scholar
26. George, M.A., Azoulay, M., Jayatirtha, H.N., Biao, Y., Burger, A., Collins, W.E. and Silberman, E., J. Crystal Growth 137, 299 (1994).Google Scholar
27. George, M.A., Chen, K-T., Collins, W.E. and Burger, A., J. Vac. Sci. Technol. B14(2),1096 (1996).Google Scholar
28. Levy, F., Mercier, A. and Voitchovsky, J-P., Solid State Comm, 15, 819 (1974).Google Scholar
29. Lund, J.C., Shah, K.S., Olschner, F., Zhang, J., Moy, L., Medrick, S. and Squillante, M.R., Nucl. Instr. and Meth. in Phys. Res. A380, 165 (1992).Google Scholar
30. Olschner, F., Lund, J.C., Shah, K.S., and Squillante, M.R., ICFA Instrum. Bull. 7,9 (1989).Google Scholar