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Probing Water Dynamics in Octahedral Molecular Sieves: High Speed 1H MAS NMR Investigations

Published online by Cambridge University Press:  26 February 2011

Todd M. Alam ,
Jason Pless  and
Tina M. Nenoff
Todd M. Alam
Affiliation:
tmalam@sandia.gov, Sandia National Laboratories, Nanostructured and Electronic Materials, 1515 Eubank SE,, MS 0886, Albuquerque, NM, NM, 87185-0886, United States, (505) 844-1225
Jason Pless
Affiliation:
djpless@sandia.gov, Sandia National Laboratories, Modelling and Simulation, Albuquerque, NM, 87185, United States
Tina M. Nenoff
Affiliation:
tmnenof@sandia.gov, Sandia National Laboratories, Surface and Interface Sciences, Albuquerque, NM, 87185-1415, United States
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Abstract

The water dynamics in molecular sieve materials are probe using high speed proton magic angle spinning NMR spectrscopy

Keywords

nuclear magnetic resonance (NMR)zeolitenanostructure
Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 984: Symposium MM – Magnetic Resonance in Material Science , 2006 , 0984-MM03-03
Copyright
Copyright © Materials Research Society 2007

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References

[1]. Nyman, M.; Tripathi, A.; Parise, J. B.; Maxwell, R. S.; Harrison, W. T. A.; Nenoff, T. M., J. Am. Chem. Soc. 123, 1529 (2001).Google Scholar
[2]. Nyman, M.; Tripathi, A.; Parise, J. B.; Maxwell, R. S.; Nenoff, T. M., J. Am. Chem. Soc. 124, 1704 (2002).Google Scholar
[3]. Goldfarb, D.; Li, H.-X.; Davis, M. E., J. Am. Chem. Soc. 114, 3690 (1992).Google Scholar
[4]. Duer, M.; He, H.; Kolodziejski, W.; Klinowski, J., J. Phys. Chem. 98, 1198 (1994).Google Scholar
[5]. Benedetto, S. Di; Chidichimo, G.; Golemme, A.; Imbardelli, D., J. Phys. Chem. 100, 8079 (1996).Google Scholar
[6]. Chidichimo, G.; Golemme, A.; Imbardelli, D.; Santoro, E., J. Phys. Chem. 94, 6826 (1990).Google Scholar
[7]. Stepanov, A. G.; Shegai, T. O.; Luzgin, M. V.; Essayem, N.; Jobic, H., J. Phys. Chem. 107, 12438 (2003).Google Scholar
[8]. Mizuno, M.; Hamada, Y.; Kitahara, T.; Suhara, M., J. Phys. Chem. A 103, 4981 (1999).Google Scholar
[9]. Wingen, A.; Basler, W.; Lechert, H., Anisotropic Motion of Water in Zeolites EMT, L, and ZSM-5 as Studied by D- and H-NMR Line Splitting. In Progress in Zeolite and Microporous Materials, Chon, H.; Ihm, S.-K.; Uh, Y.S., Eds. Elsevier Science B. V.: 1997; Vol.105, pp 495.Google Scholar
[10]. Kobe, J. M.; Gluszak, T. J.; Dumesic, J. A.; Root, T. W., J. Phys. Chem. 99, 5485 (1995).Google Scholar
[11]. Bielecki, A.; Burum, D. P., Journal of Magnetic Resonance, Series A 116, 215 (1995).Google Scholar
[12]. Takahashi, T.; Kawashima, H.; Sugisawa, H.; Baba, T., Solid State Nuclear Magnetic Resonance 15, 119 (1999).Google Scholar
[13]. Schnell, I.; Spiess, H. W., J. Mag. Res. 151, 153 (2001).Google Scholar
[14]. Holland, G. P.; Cherry, B. R.; Alam, T. M., J. Magn. Reson. 167, 161 (2004).Google Scholar
[15]. Alam, T. M.; Nyman, M.; Cherry, B. R.; Segall, J. M.; Lybarger, L. E., J. Am. Chem. Soc. 126, 5610 (2004).Google Scholar
[16]. Abragam, A., Principles of Nuclear Magnetism. Clarendon Press: Oxford, 1961; p 599.Google Scholar
[17]. Batamack, P.; Dorémieux-Morin, C.; Vincent, R.; Fraissard, J., Chem. Phys. Lett. 180, 545 (1991).Google Scholar
[18]. Batamack, P.; Dorémieux-Morin, C.; Vincent, R.; Fraissard, J., J. Phys. Chem. 97, 9779 (1993).Google Scholar
[19]. Udea, T.; Nakamura, N., J. Phys. Chem. B 107, 13681 (2003).Google Scholar
[20]. Tritt-Goc, J.; Pislewski, N., Molecular Physics 83, 949 (1994).Google Scholar