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Quantitative Electron Diffraction for Crystal Structure Determination

Published online by Cambridge University Press:  31 January 2011

Peter Oleynikov
Affiliation:
oleyniko@struc.su.se, Stockholm University, Structural Chemistry, Stockholm, Sweden
Daniel Grüner
Affiliation:
danielg@inorg.su.se, Stockholm University, Inorganic Chemistry, Stockholm, Sweden
Daliang Zhang
Affiliation:
Daliangz@struc.su.se, Stockholm University, Structural Chemistry, Stockholm, Sweden
Junliang Sun
Affiliation:
Junliangs@struc.su.se, Stockholm University, Structural Chemistry, Stockholm, Sweden
Xiaodong Zou
Affiliation:
zou@struc.su.se, Stockholm University, Structural Chemistry, Stockholm, Sweden
Sven Hovmöller
Affiliation:
svenh@struc.su.se, Stockholm University, Structural Chemistry, Stockholm, Sweden
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Abstract

We present a quantitative investigation of data quality using electron precession, compared to standard selected-area electron diffraction (SAED). Data can be collected on a CCD camera and automatically extracted by computer. The critical question of data quality is addressed – can electron diffraction data compete with X-ray diffraction data in terms of resolution, completeness and quality of intensities?

Type
Research Article
Copyright
Copyright © Materials Research Society 2009

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References

1. Weirich, T., Ramlau, R., Simon, A., Zou, X.D. and Hovmöller, S., Nature 382, 144146 (1996).Google Scholar
2. Vincent, R. and Midgley, P. A., Ultramicroscopy 53, 271 (1994).Google Scholar
3. Baerlocher, C., Gramm, F., Massüger, L., McCusker, L.B., He, Z.B., Hovmöller, S. and Zou, X.D., Science 315, 11131116 (2007).Google Scholar
4. Zou, X.D., Mo, Z.M., Hovmöller, S., Li, X.Z. and Kuo, K., Acta Cryst. A59, 526539 (2003).Google Scholar
5. Kolb, U., Gorelik, T., Hübel, C., Otten, M.T. and Hubert, D., Ultramicroscopy 107, 507513 (2007).Google Scholar
6. Hu, J.J., Li, F.H. and Fan, H.F.. Ultramicroscopy 41, 387397 (1992).Google Scholar
7. Wang, D.N., Hovmöller, S., Kihlborg, L. and Sundberg, M., Ultramicroscopy 25, 303316 (1988).Google Scholar
8. Bhide, V., Gasparin, M.. Acta Cryst. B35, 13181321 (1979).Google Scholar
9. Zou, X.D., Sukharev, Y. and Hovmöller, S., Ultramicroscopy 49, 147158 (1993).Google Scholar
10. Altomare, A., Burla, M.C., Camalli, M., Cascarano, G., Giacovazzo, C., Guagliardi, A., Moliterni, A.G.G., Polidori, G. and Spagna, R.. J. Appl. Cryst. 32, 115118 (1999).Google Scholar
11. Sheldrick, G.M., Acta Crystallogr. A64, 112122 (2008).Google Scholar
12. Gjønnes, J. and Moodie, A.F., Acta Crystallogr. 19, 6567 (1965).Google Scholar
13. Oleynikov, P., Analitex, Sweden, http://www.analitex.com/.Google Scholar
14. Georgieva, D.G., Jiang, L., Zandbergen, H.W. and Abrahams, J.P., Acta Crystallogr. D64, (2009) (in press).Google Scholar