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Synthesis of new hybrid material based on copolymer and Pd-nanoparticles.

Published online by Cambridge University Press:  17 December 2012

M. Ugalde ,
E. Chavira ,
M. T. Ochoa-Lara ,
M. A. Canseco ,
E.A. Zaragoza-Contreras ,
C. Quintanar  and
M. Gutiérrez-Nava
M. Ugalde*
Affiliation:
Laboratorio Nacional de Nanotecnología, Centro de Investigación en Materiales Avanzados, S.C., Ave. Miguel de Cervantes #120, C.P. 31109, Chihuahua, Chih., MÉXICO. Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, A. P. 70-360, 04510 México, D. F., MÉXICO.
E. Chavira
Affiliation:
Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, A. P. 70-360, 04510 México, D. F., MÉXICO.
M. T. Ochoa-Lara
Affiliation:
Laboratorio Nacional de Nanotecnología, Centro de Investigación en Materiales Avanzados, S.C., Ave. Miguel de Cervantes #120, C.P. 31109, Chihuahua, Chih., MÉXICO.
M. A. Canseco
Affiliation:
Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, A. P. 70-360, 04510 México, D. F., MÉXICO.
E.A. Zaragoza-Contreras
Affiliation:
Laboratorio Nacional de Nanotecnología, Centro de Investigación en Materiales Avanzados, S.C., Ave. Miguel de Cervantes #120, C.P. 31109, Chihuahua, Chih., MÉXICO.
C. Quintanar
Affiliation:
Facultad de Ciencias, Universidad 3000 Circuito Exterior S/N, C.P. 04510 Ciudad Universitaria, MÉXICO.
M. Gutiérrez-Nava
Affiliation:
CIATEQ A.C., Centro de Tecnología Avanzada, , Carretera México Toluca Km. 53.5, en Fraccionamiento Parque Industrial y Tecnológico, Ex Hacienda Doña Rosa, L. 11, Mz. 3, Toluca, Estado de México, MÉXICO C.P. 52000.
*
*E-mail: magali.ugalde@cimav.edu.mx
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Abstract

In this work, the synthesis of new hybrid material based on a poly (buthyl acrylate –co- vinyl formamide) copolymer using the emulsion polymerization and doped with Pd, is discussed. The copolymer structure was confirmed by FT-IR. Afterwards, Pd nanocrystals previously synthesized, resulting on a spherical shape of ~ 5 nm, as measured by High-resolution transmission electron microscopy (HR-TEM), were deposited on the structure of the organic material. The films were analyzed using AFM and Scanning electron microscopy (SEM), giving rise to a hybrid material that could be applied in areas such as nanolithography, catalysis, and sensors.

Keywords

PolymersensorScanning Electron Microscopy (SEM)
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1483: Symposium S – New Trends in Polymer Chemistry and Characterization , 2012 , imrc12-1483-s5b-p029
Copyright
Copyright © Materials Research Society 2012 

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References

REFERENCES

Brennan, A.B., Wilkes, G.L., Polymer, 32(4), 733–739 (1991),CrossRefGoogle Scholar
Zhao, Wenru, Gu, Jinlou, Zhang, Lingxia, Chen, Hangrong, and Shi, Jianlin J. Am. Chem. Soc., 127, (25) 8916–8917(2005).CrossRefGoogle Scholar
Houbertz, R., Domann, G., Cronauer, C., Schmitt, A., Martin, H., Park, J.-U., Fröhlich, L., Buestrich, R., Popall, M., Streppel, U., Dannberg, P., Wächter, C., Bräuer, A. Thin Solid Films Volume 442,(1–2) 194–200 (2003).CrossRefGoogle Scholar
Kros, A., van Hövel, S.W.F.M., Nolte, R.J.M., Sommerdijk, N.A.J.M., Sensors and Actuators B: Chemical, Volume 80, (3–1) 229–233 (2001).CrossRefGoogle Scholar
Sin, A., Odier, P., Adv. Mater. 12(9), 649–652 (2000).3.0.CO;2-K>CrossRefGoogle Scholar
Ugalde, M., Chavira, E., Ochoa-Lara, M. T., Carlos Quintanar Journal of Nano Research 14, 93–103 (2011).CrossRefGoogle Scholar
Maxwell, Ian. A., Napper, Donald H., Gilbert, Robert G., J. Chem. SOC., Faraday Trans. 1, ,83, 1449–1467 (1987).CrossRefGoogle Scholar
Bronstein, Lyudmila, Kramer, Eckhard, Berton, Beate, Burger, Christian, Forster, Stephan, and Antonietti, Markus Chem. Mater, (11), 1402–1405 (1999).CrossRefGoogle Scholar