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Transformation of carbon onions under high pressure and shear deformation in diamond anvil cell

Published online by Cambridge University Press:  23 August 2012

A.N. Kirichenko ,
A.K. Aseev ,
V.N. Denisov ,
I. Perezhogin ,
B.A. Kulnitskiy ,
A.A. Nuzhdin  and
V.D. Blank
A.N. Kirichenko
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation.
A.K. Aseev
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation.
V.N. Denisov
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation. Institute of spectroscopy RAS, 5 Fizicheskaya street, Troitsk, Moscow region, 142190 Russian Federation.
I. Perezhogin
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation.
B.A. Kulnitskiy
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation.
A.A. Nuzhdin
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation.
V.D. Blank
Affiliation:
FSBI TISNCM, 7a Centralnaya street, Troitsk, Moscow region, 142190, Russian Federation.
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Abstract

The carbon onions have been treated in a shear diamond anvil cell under pressure up to 43 GPa and shear deformation up to 2000. The recovered samples have been investigated by the Transmission Electron Microscopy (TEM) and the UV and visible Raman spectroscopy. The carbon onions was stable at pressure up to 30 GPa and 400 shear. Bigger shear deformation at pressures exceeding 30 GPa leads to the amorphous carbon. At 43 GPa shear deformation leads to transformation of onions to DLC.

Keywords

nanostructurescanning electron microscopy (SEM)Raman spectroscopy
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1452: Symposium FF – Nanodiamond Particles and Related Materials--From Basic Science to Applications , 2012 , mrss12-1452-ff08-02
Copyright
Copyright © Materials Research Society 2012

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References

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