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Powder diffraction investigations of some organic hydrochlorides

Published online by Cambridge University Press:  01 March 2012

B. Lasocha
Affiliation:
Medical College, Faculty of Medicine, Jagiellonian University, Św. Anny 12, 31-008 Kraków, Poland
B. Gawel
Affiliation:
Faculty of Chemistry, Jagiellonian University, Ingardena 3, 30-060 Kraków, Poland
W. Lasocha*
Affiliation:
Faculty of Chemistry, Jagiellonian University, Ingardena 3, 30-060 Kraków, Polandand Institute of Catalysis and Surface Chemistry PAS, Niezapominajek 8, 30-039 Kraków, Poland
*
a)The author to whom correspondence should be addressed.

Abstract

Amantadine hydrochloride, p-aminophenol hydrochloride, and methylamine hydrochloride, compounds often studied in pharmacology, were investigated by means of powder diffractometry. The chemical formula of the first compound is C10H17N HCl and crystallizes in the monoclinic system, space group C2∕c (15) with lattice parameters a=2.0279(6) nm, b=1.1171(2) nm, c=9.759(4) nm, and β=109.00(3)°. p-Aminophenol hydrochloride C6H7NO HCl crystallizes in the orthorhombic system, space group P222 with lattice parameters a=0.6619(2) nm, b=0.88461(2) nm, and c=0.6101(2) nm. Methylamine hydrochloride CH5N∙HCl crystallizes in the tetragonal system, space group P4∕nmm (129) with lattice parameters a=b=0.6068(1) nm and c=0.50689(8) nm.

Type
New Diffraction Data
Copyright
Copyright © Cambridge University Press 2006

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References

Appelman, D. E., Evans, H. T., and Handwerker, D. S. (1966). “Program X-ray, Geological Survey.”Google Scholar
Bélanger-Gariépy, F., Brisse, F., Harvey, P. D., Butler, I. S., and Gilson, D. F. R. (1987). “Structure of adamantanamine hydrochloride at 143 K,” Acta Crystallogr. ACSCEE 43, 756759.Google Scholar
ICDD (2006). “Powder Diffraction File,” International Centre for Diffraction Data, edited by Frank McClune, 12 Campus Boulevard, Newtown Square, PA 19073-3272.Google Scholar
Lasocha, W. and Lewinski, K. (1994). “PROSZKI—a system of programs for powder diffraction data analysis,” J. Appl. Crystallogr. JACGAR 10.1107/S002188989400066X 27, 437438.CrossRefGoogle Scholar
Simpson, L. L. (1983). “Ammonium chloride and methylamine hydrochloride antagonize clostridial neurotoxins,” J. Pharmacol. Exp. Ther. JPETAB 225, 546552.Google ScholarPubMed
Smith, G. S. and Snyder, R. L. (1979). “F N: A criterion for rating powder diffraction patterns and evaluating the reliability of powder-pattern indexing,” J. Appl. Crystallogr. JACGAR 10.1107/S002188987901178X 12, 6065.CrossRefGoogle Scholar
Song, H. and Chen, T. S. (2001). “p-Aminophenol-induced liver toxicity: Tentative evidence of a role for acetaminophen,” J. Biochem. Mol. Toxicol. JBMTFQ 15, 3440.3.0.CO;2-U>CrossRefGoogle ScholarPubMed
Sonneveld, E. J. and Visser, J. W. (1975). “Automatic collection of powder data from photographs,” J. Appl. Crystallogr. JACGAR 10.1107/S0021889875009417 8, 17.CrossRefGoogle Scholar
Stammler, M. (1967). “Polymorphism of salts containing complex ions—: The halides of ammonium and methyl-substituted ammonium,” J. Inorg. Nucl. Chem. JINCAO 29, 22032221.CrossRefGoogle Scholar
Visser, J. W. (1969). “A fully automatic program for finding the unit cell from powder data,” J. Appl. Crystallogr. JACGAR 10.1107/S0021889869006649 2, 8995.CrossRefGoogle Scholar
Werner, P.-E., Eriksson, L., and Westdahl, M. (1985). “TREOR, a semi-exhaustive trial-and-error powder indexing program for all symmetries,” J. Appl. Crystallogr. JACGAR 10.1107/S0021889885010512 18, 367370.CrossRefGoogle Scholar
Wolf, P. M. de (1972). “The definition of the indexing figure of merit M20,” J. Appl. Crystallogr. JACGAR 10.1107/S002188987200932X 5, 243.CrossRefGoogle Scholar