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Powder X-ray characterization of djenkolic acid

Published online by Cambridge University Press:  05 March 2012

Petr Melnikov*
Affiliation:
CCET-UFMS, 79070-900 Cidade Universita´ria, s/n, Campo Grande, MS, Brazil
Alexandre Cuin*
Affiliation:
Department of General and Inorganic Chemistry, Institute of Chemistry-UNESP, P.O. Box 355, 14800-970 Francisco Degni, s/n, Araraquara, SP, Brazil
Pedro P. Corbi*
Affiliation:
Department of General and Inorganic Chemistry, Institute of Chemistry-UNESP, P.O. Box 355, 14800-970 Francisco Degni, s/n, Araraquara, SP, Brazil
Maurício Cavicchioli*
Affiliation:
Department of General and Inorganic Chemistry, Institute of Chemistry-UNESP, P.O. Box 355, 14800-970 Francisco Degni, s/n, Araraquara, SP, Brazil
Antonio C. Massabni*
Affiliation:
Department of General and Inorganic Chemistry, Institute of Chemistry-UNESP, P.O. Box 355, 14800-970 Francisco Degni, s/n, Araraquara, SP, Brazil
*
a)Electronic mail: petrmelnikov@yahoo.com
b)Electronic mail: alexcuin@iq.unesp.br
c)Electronic mail: pedrocorbi@yahoo.com
d)Electronic mail: maurcavi@iq.unesp.br
e)Electronic mail: massabni@iq.unesp.br

Abstract

X-ray powder diffraction data for the orthorhombic natural amino acid djenkolic acid, C7H14N2O4S2, is described in this paper. The orthorhombic cell parameters are: a=8.12 Å, b=12.16 Å, and c=5.38 Å

Type
New Diffraction Data
Copyright
Copyright © Cambridge University Press 2001

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References

Armstrong, M. D., and Vigneaud, V. (1947). “A new synthesis of djenkolic acid,” J. Biol. Chem. JBCHA3 168, 373377. jbc, JBCHA3 CrossRefGoogle ScholarPubMed
Bigoli, F., Lanfranchi, M., Leporati, E., Nardeli, M., and Pellinghelli, M. A. (1982). “The structure of S,S-methylenebis(L-cysteine) monohydrochloride,” Acta Crystallogr., Sect. B: Struct. Crystallogr. Cryst. Chem. ACBCAR B38, 498502. acb, ACBCAR CrossRefGoogle Scholar
Dictionary of Natural Products (1997). CD-ROM Database, Version 6 (Chapman & Hall, London).Google Scholar
Eli Lilly & Co. (private communication).Google Scholar
Jarusiripipat, C., Shapiro, J. I., and Chan, L. (1988). “Djenkolic acid induces acute renal failure,” Kidney Int. ZZZZZZ 33, 359359. 5t2, ZZZZZZ Google Scholar
Kerr, K. A., and Ashmore, J. P. (1973). “Structure and conformation of orthorhombic L-cysteine,” Acta Crystallogr., Sect. B: Struct. Crystallogr. Cryst. Chem. ACBCAR B29, 21242127. acb, ACBCAR CrossRefGoogle Scholar
Powder Diffraction File Database (1994). 08-0660 (JCPDS-ICDD).Google Scholar