Hostname: page-component-78c5997874-m6dg7 Total loading time: 0 Render date: 2024-11-14T23:30:30.237Z Has data issue: false hasContentIssue false
  • English
  • Français

Texture and microstructure analysis with high-energy synchrotron radiation

Published online by Cambridge University Press:  06 March 2012

Hans J. Bunge
Hans J. Bunge*
Affiliation:
Department of Physics and Physical Technologies, TU Clausthal, Leibniz str. 4, D-38678, Clausthal-Zellerfeld, Germany
*
a)Electronic mail: hans.bunge@t-online.de
Get access Rights & Permissions [Opens in a new window]

Abstract

Diffraction of high-energy synchrotron radiation with wavelengths in the range of 0.1 Å, provided by the beamline BW5 at HASYLAB in Hamburg, was used to measure textures (orientation distribution) and microstructures (spatial distribution) of the crystallites in various polycrystalline materials. In order to achieve extremely high angular-combined with very high lateral resolution a continuous sweeping technique with an area detector was employed. This technique “images” three different types of two-dimensional sections and projections of the six-dimensional orientation–location space onto the area detector. In many cases the orientations and locations of all individual grains of the sample can thus be seen simultaneously. The high penetration depth of this radiation in the range of several centimeters (comparable with that of neutrons) allows investigating big or capsulated samples. Examples are given of grain-resolved recrystallization textures, a soldering seam, a filled beverage can, and the orientation distribution of kamacite lamellae in an iron meteorite, elucidating the orientation relationship of the γ→α transformation in iron.

Type
Technical Articles
Information
Powder Diffraction , Volume 19 , Issue 1 , March 2004 , pp. 60 - 64
Copyright
Copyright © Cambridge University Press 2004

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Bunge, H. J. (1982). Texture Analysis in Materials Science (Butterworths, London).Google Scholar
Bunge, H. J. (2003). “Über Meteoriten, Bierdosen und Synchrotronstrahlen,” TU Contact (Clausthal)ZZZZZZ 12, 27–31.Google Scholar
Bunge, H. J., Morris, P. R., and Nauer-Gerhardt, C. N. (1989). “ODF-analysis of multipeak textures,” Textures Microstruct. TEMIDK 11, 1–22. tem, TEMIDK CrossRefGoogle Scholar
Bunge, H. J.and Schwarzer, R. A. (2001). “Orientation stereology—A new branch in texture research,” Adv. Eng. Mater.ZZZZZZ 3, 25–39.3.0.CO;2-8>CrossRefGoogle Scholar
Bunge, H. J., Wcislak, L., Klein, H., Garbe, U., and Schneider, J. R. (2002). “Texture and microstructure analysis with high-energy synchrotron radiation,” Adv. Eng. Mater.ZZZZZZ 4, 300–304.Google Scholar
Bunge, H. J., Wcislak, L., Klein, H., Garbe, U., and Schneider, J. R. (2003). “Texture and microstructure imaging in six dimensions with high-energy synchrotron radiation,” J. Appl. Crystallogr. JACGAR 36, 1240–1255. acr, JACGAR Google Scholar
Bunge, H. J., Weiss, W., Klein, H., Wcislak, L., Garbe, U., and Schneider, J. R. (2003). “Orientation relationship of Widmannstätten plates in an iron meteorite measured with high-energy synchrotron radiation,” J. Appl. Crystallogr. JACGAR 36, 137–140. acr, JACGAR Google Scholar
Bouchard, R., Hupfeld, D., Lippmann, T., Neuefeind, J., Neumann, H. B., Poulsen, H. F., Rütt, U., Schmldt, T., Schneider, J. R., Sussenbach, J., and von Zimmermann, M. (1998). “Triple-crystal diffractometer for high-energy synchrotron radiation at the HASYLAB high-field wiggler beamline BW5,” J. Synchrotron Radiat. JSYRES 5, 90–101. jsy, JSYRES CrossRefGoogle ScholarPubMed
Klein, H.and Bunge, H. J. (1999). “Location resolved texture analysis,” Z. Metallkd. ZEMTAE 90, 103–110. zem, ZEMTAE Google Scholar
Wcislak, L., Klein, H., Bunge, H. J., Garbe, U., Tschentscher, T., and Schneider, J. R. (2002). “Texture analysis with high-energy synchrotron radiation,” J. Appl. Crystallogr. JACGAR 35, 82–95. acr, JACGAR Google Scholar
Wassermann, G. and Grewen, J. (1962). Texturen Metallischer Werkstoffe (Springer-Verlag, Berlin).Google Scholar
Weiss, W.and Bunge, H. J. (2001). “Diffraction contrast in X-ray radiographic images of octahedric meteorites,” J. Appl. Crystallogr. JACGAR 34, 566–572. acr, JACGAR Google Scholar