Hostname: page-component-78c5997874-g7gxr Total loading time: 0 Render date: 2024-11-10T15:41:35.515Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray powder diffraction data for monosodium salt azobarbituric acid dihydrate [C8H5N6O6Na.2H2O]

Published online by Cambridge University Press:  04 August 2014

J. Maixner ,
J. Rohlíček ,
Č. Florián ,
J. Vyňuchal  and
F. Alafid
J. Maixner*
Affiliation:
Central Laboratories, Institute of Chemical Technology Prague, Technická 5, 166 28 Prague 6, Czech Republic
J. Rohlíček
Affiliation:
Institute of Physics AS CR,v.v.i., Na Slovance 2, 182 21 Prague 8, Czech Republic
Č. Florián
Affiliation:
Synthesia a.s., Pardubice, Semtín 103, CZ-532 17 Pardubice, Czech Republic
J. Vyňuchal
Affiliation:
Synthesia a.s., Pardubice, Semtín 103, CZ-532 17 Pardubice, Czech Republic
F. Alafid
Affiliation:
Faculty of Chemical Technology, Institute of Organic Chemistry and Technology, University of Pardubice, Studentská 95, 53210 Pardubice, Czech Republic
*
a) Author to whom correspondence should be addressed. Electronic mail: jaroslav.maixner@vscht.cz
Get access Rights & Permissions [Opens in a new window]

Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for a sodium azobarbituric acid dihydrate are presented [a = 3.546 (1) Å, b = 9.210 (2) Å, c = 9.738 (4) Å, α = 104.07 (4)°, β = 98.09 (6)°, γ = 98.80 (2)°, unit-cell volume V = 299.6 Å3, Z = 1, and space group P − 1]. All the measured lines were indexed. No detectable impurities were observed.

Keywords

X-ray powder diffractionpigmentssodium azobarbituric acid dihydrate
Type
New Diffraction Data
Information
Powder Diffraction , Volume 29 , Issue 4 , December 2014 , pp. 383 - 384
Copyright
Copyright © International Centre for Diffraction Data 2014 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Allen, F. H. (2002). “The Cambridge Structural Database: a quarter of a million crystal structures and rising,” Acta Crystallogr. B 58, 380–388.CrossRefGoogle ScholarPubMed
Boultif, A. and Louër, D. (2004). “Powder pattern indexing with the dichotomy method,” J. Appl. Crystallogr. 37, 724–731.CrossRefGoogle Scholar
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern,” J. Appl. Crystallogr. 1, 108–113.CrossRefGoogle Scholar
ICDD (2012). Powder Diffraction File, edited by Kabekkodu, S., International Centre for Diffraction Data, 12 Campus Boulevard, Newton Square, Pennsylvania 19073-3272.Google Scholar
Smith, G. S. and Snyder, R. L. (1979). “ F N: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar