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X-ray powder diffraction investigations of phenol derivatives

Published online by Cambridge University Press:  06 March 2012

A. Rafalska-Lasocha ,
B. Włodarczyk-Gajda ,
M. Grzywa  and
W. Lasocha
A. Rafalska-Lasocha
Affiliation:
Faculty of Chemistry Jagiellonian University, Ingardena 3, 30-060 Krakow, Poland
B. Włodarczyk-Gajda
Affiliation:
Faculty of Chemistry Jagiellonian University, Ingardena 3, 30-060 Krakow, Poland
M. Grzywa
Affiliation:
Faculty of Chemistry Jagiellonian University, Ingardena 3, 30-060 Krakow, Poland
W. Lasocha*
Affiliation:
Faculty of Chemistry Jagiellonian University, Ingardena 3, 30-060 Krakow, Poland
*
a)Author to whom the correspondence should be addressed; electronic mail: lasocha@chemia.uj.edu.pl
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Abstract

The X-ray powder diffraction patterns of three phenol derivatives—2-chlorophenol, 2,6-dichloro-4-nitrophenol, and 2,6-dichloro-phenoloindophenol tetrahydrate—were collected and the lattice parameters of these compounds were determined. The measurement for 2-chlorophenol was carried out at 250 K in a low-temperature chamber; this compound crystallizes in hexagonal system with a=1.59602(8) nm, c=0.59761(7) nm, space group P6 or P63/m. Investigated at room temperature, 2,6-dichloro-4-nitrophenol and 2,6-dichloro-phenoloindophenol tetrahydrate crystallize in the triclinic system with the unit cell parameters refined to a=0.8169(2) nm, b=1.6637(6) nm, c=0.7440(1) nm, α=96.6(3)°, β=116.19(2)°, γ=78.68°, and space group P-1(2), and a=0.7792(3) nm, b=1.2795(4) nm, c=0.7256(3) nm, α=91.17(5)°, β=96.93(4)°, γ=85.41(3)°, and space group P-1(2), respectively. © 2004 International Centre for Diffraction Data.

Type
New Diffraction Data
Information
Powder Diffraction , Volume 19 , Issue 3 , September 2004 , pp. 292 - 295
Copyright
Copyright © Cambridge University Press 2004

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