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Crystal Data of Diltiazem Hydrochloride C22H26N2O4S·HCl

Published online by Cambridge University Press:  10 January 2013

I. Mayer
Affiliation:
Department of Inorganic and Analytical Chemistry, Hebrew University, Jerusalem, Israel
S. Cohen
Affiliation:
Department of Inorganic and Analytical Chemistry, Hebrew University, Jerusalem, Israel
L. Tsamir
Affiliation:
Abic Pharmaceutical & Chemical Industries, Netanya, Israel

Abstract

X-ray powder diffraction analysis of Diltiazem Hydrochloride C22H26N2O4S·HCl reveals that the compound crystallizes in an orthorhombic unit cell with the powder data unit cell parameters of a=9.08(1), b=42.09(4), c=6.03(1) Å, V=2305 Å3. The unit cell dimensions determined by single crystal diffraction analysis agree well with those of powder diffraction analysis. Samples prepared under different crystallization conditions yielded the same powder patterns.

Type
Research Article
Copyright
Copyright © Cambridge University Press 1990

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